(4R,5S)-5-(tert-butoxycarbonyl)-1-(9-phenylfluoren-9-yl)-4-benzylimidazolidin-2-one

Base Information

Chemical Name:(4R,5S)-5-(tert-butoxycarbonyl)-1-(9-phenylfluoren-9-yl)-4-benzylimidazolidin-2-one
CAS No.:128657-45-4
Molecular Formula:C₃₄H₃₂N₂O₃
Molecular Weight:516.64
Hs Code.:

Synonyms:(4R,5S)-5-(tert-butoxycarbonyl)-1-(9-phenylfluoren-9-yl)-4-benzylimidazolidin-2-one

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Chemical Property of (4R,5S)-5-(tert-butoxycarbonyl)-1-(9-phenylfluoren-9-yl)-4-benzylimidazolidin-2-one

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Technology Process of (4R,5S)-5-(tert-butoxycarbonyl)-1-(9-phenylfluoren-9-yl)-4-benzylimidazolidin-2-one

There total 1 articles about (4R,5S)-5-(tert-butoxycarbonyl)-1-(9-phenylfluoren-9-yl)-4-benzylimidazolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 128576-57-8,128576-84-1
(S)-2-Benzyl-3-(9-phenyl-9H-fluoren-9-ylamino)-succinic acid 4-tert-butyl ester

: 128576-58-9
(4S,5S)-5-(tert-butoxycarbonyl)-1-(9-phenylfluoren-9-yl)-4-benzylimidazolidin-2-one

: 128657-45-4
(4R,5S)-5-(tert-butoxycarbonyl)-1-(9-phenylfluoren-9-yl)-4-benzylimidazolidin-2-one

Guidance literature:: With diphenyl-phosphinic acid; triethylamine; In acetonitrile; at 60 ℃; for 15h;
DOI:10.1021/jo00304a011

Reference yield: 98.0%

: 128657-45-4
(4R,5S)-5-(tert-butoxycarbonyl)-1-(9-phenylfluoren-9-yl)-4-benzylimidazolidin-2-one

: 128657-46-5
(4S,5R)-4-carboxy-5-benzylimidazolidin-2-one

Guidance literature:: With trifluoroacetic acid; In dichloromethane; for 17h; Ambient temperature;
DOI:10.1021/jo00304a011

Reference yield:

: 128657-45-4
(4R,5S)-5-(tert-butoxycarbonyl)-1-(9-phenylfluoren-9-yl)-4-benzylimidazolidin-2-one

: 128576-79-4
(4S,5R)-5-benzyl-4-(methoxycarbonyl)imidazolidin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / trifluoroacetic acid / CH₂Cl₂ / 17 h / Ambient temperature

2: thionyl chloride / 12 h / Ambient temperature

With thionyl chloride; trifluoroacetic acid; In dichloromethane;
DOI:10.1021/jo00304a011