(R)-2-hydroxy-2-phenylethyl 4-[4-(6-acryloyloxyhexyloxy)benzoyloxy]cinnamate

Base Information

Chemical Name:(R)-2-hydroxy-2-phenylethyl 4-[4-(6-acryloyloxyhexyloxy)benzoyloxy]cinnamate
CAS No.:642471-42-9
Molecular Formula:C₃₃H₃₄O₈
Molecular Weight:558.628
Hs Code.:

Synonyms:(R)-2-hydroxy-2-phenylethyl 4-[4-(6-acryloyloxyhexyloxy)benzoyloxy]cinnamate

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Chemical Property of (R)-2-hydroxy-2-phenylethyl 4-[4-(6-acryloyloxyhexyloxy)benzoyloxy]cinnamate

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Technology Process of (R)-2-hydroxy-2-phenylethyl 4-[4-(6-acryloyloxyhexyloxy)benzoyloxy]cinnamate

There total 7 articles about (R)-2-hydroxy-2-phenylethyl 4-[4-(6-acryloyloxyhexyloxy)benzoyloxy]cinnamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: (R)-4-(4-(6-acryloyloxyhexyloxy)benzoyloxy)cinnamic acid 2-(tetrahydropyran-2-yloxy)-2-phenyl-ethyl ester

: 642471-42-9
(R)-2-hydroxy-2-phenylethyl 4-[4-(6-acryloyloxyhexyloxy)benzoyloxy]cinnamate

Guidance literature:: With pyridinium p-toluenesulfonate; 4-methoxy-phenol; In ethanol; at 55 ℃; for 20h;

Reference yield:

: 83883-26-5
4-{[6-(acryloyloxy)hexyl]oxy}benzoic acid

: 642471-42-9
(R)-2-hydroxy-2-phenylethyl 4-[4-(6-acryloyloxyhexyloxy)benzoyloxy]cinnamate

Guidance literature:: Multi-step reaction with 4 steps

1: N,N'-dicyclohexylcarbodiimide; 4-(dimethylamino)pyridine / CH₂Cl₂ / 20 °C

2: 12.7 g / pyridinium 4-toluenesulfonate / ethanol / 13 h / 60 °C

3: N,N'-dicyclohexylcarbodiimide; 4-(dimethylamino)pyridine / CH₂Cl₂

4: pyridinium 4-toluenesulfonate / ethanol / 60 °C

With dmap; pyridinium p-toluenesulfonate; dicyclohexyl-carbodiimide; In ethanol; dichloromethane;
DOI:10.1080/15421400600700299

Reference yield:

: 642471-45-2
ethoxymethyl 4-hydroxycinnamate

: 642471-42-9
(R)-2-hydroxy-2-phenylethyl 4-[4-(6-acryloyloxyhexyloxy)benzoyloxy]cinnamate

Guidance literature:: Multi-step reaction with 4 steps

1: N,N'-dicyclohexylcarbodiimide; 4-(dimethylamino)pyridine / CH₂Cl₂ / 20 °C

2: 12.7 g / pyridinium 4-toluenesulfonate / ethanol / 13 h / 60 °C

3: N,N'-dicyclohexylcarbodiimide; 4-(dimethylamino)pyridine / CH₂Cl₂

4: pyridinium 4-toluenesulfonate / ethanol / 60 °C

With dmap; pyridinium p-toluenesulfonate; dicyclohexyl-carbodiimide; In ethanol; dichloromethane;
DOI:10.1080/15421400600700299