2,3,5-tri-O-acetyl-D-ribopyranosyl bromide

Base Information

• Chemical Name: 2,3,5-tri-O-acetyl-D-ribopyranosyl bromide
• CAS No.: 50730-32-0
• Molecular Formula: C₁₁H₁₅BrO₇
• Molecular Weight: 339.14

Synonyms:2,3,5-tri-O-acetyl-D-ribopyranosyl bromide

Chemical Property of 2,3,5-tri-O-acetyl-D-ribopyranosyl bromide

Chemical Property:

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Technology Process of 2,3,5-tri-O-acetyl-D-ribopyranosyl bromide

There total 2 articles about 2,3,5-tri-O-acetyl-D-ribopyranosyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ Tri-O-acetyl-β-D-arabinosylbromid (3056-11-9,3068-29-9,3068-30-2,3068-31-3,4049-35-8,4099-16-5,14227-90-8,39524-37-3,39524-39-5,50730-32-0,50837-92-8,51830-02-5,55555-59-4,65914-26-3,75247-31-3,102339-91-3,103530-43-4,113889-50-2,138514-72-4,138514-73-5)

Guidance literature:

Triacetyl-D-arabinose;

Reference yield:

→ Tri-O-acetyl-α-D-xylopyranosylbromid (3056-11-9,3068-29-9,3068-30-2,3068-31-3,4049-35-8,4099-16-5,14227-90-8,39524-37-3,39524-39-5,50730-32-0,50837-92-8,51830-02-5,55555-59-4,65914-26-3,75247-31-3,102339-91-3,103530-43-4,113889-50-2,138514-72-4,138514-73-5)

Guidance literature:

Tetra-O-acetyl-β-D-xylopyranose, gasf. HBr, Eg. (0grad, 2h);

Reference yield: 90.1%

2,3,5-tri-O-acetyl-D-ribopyranosyl bromide (50730-32-0) → 3,4-di-O-acetyl-D-arabinal (3152-43-0,3945-17-3,3945-18-4,86257-92-3,89921-34-6,89921-35-7,101052-70-4)

Guidance literature:

With silver-graphite; zinc; In tetrahydrofuran; at -20 - 25 ℃; for 0.333333h;

DOI:10.1039/c39860001149

Downstream raw materials:

3,4-di-O-acetyl-D-xylal

Acetic acid (3S,6R)-6-methoxy-3,6-dihydro-2H-pyran-3-yl ester

3,4-di-O-acetyl-D-arabinal

Acetic acid (1R,4R,9R,10R)-7-methyl-3,5,8,11-tetraoxa-tricyclo[5.3.2.0^4,9]dodec-10-yl ester

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