Phosphoric acid (1S,2R,3R,4R,5R,6S)-2,5-bis-benzyloxy-3,4-bis-(bis-benzyloxy-phosphoryloxy)-6-fluoro-cyclohexyl ester (R)-2,3-dibutoxy-propyl ester

Base Information

Chemical Name:Phosphoric acid (1S,2R,3R,4R,5R,6S)-2,5-bis-benzyloxy-3,4-bis-(bis-benzyloxy-phosphoryloxy)-6-fluoro-cyclohexyl ester (R)-2,3-dibutoxy-propyl ester
CAS No.:208844-99-9
Molecular Formula:C₅₉H₇₂FO₁₆P₃
Molecular Weight:1149.13
Hs Code.:

Phosphoric acid (1S,2R,3R,4R,5R,6S)-2,5-bis-benzyloxy-3,4-bis-(bis-benzyloxy-phosphoryloxy)-6-fluoro-cyclohexyl ester (R)-2,3-dibutoxy-propyl ester

Synonyms:Phosphoric acid (1S,2R,3R,4R,5R,6S)-2,5-bis-benzyloxy-3,4-bis-(bis-benzyloxy-phosphoryloxy)-6-fluoro-cyclohexyl ester (R)-2,3-dibutoxy-propyl ester

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Chemical Property of Phosphoric acid (1S,2R,3R,4R,5R,6S)-2,5-bis-benzyloxy-3,4-bis-(bis-benzyloxy-phosphoryloxy)-6-fluoro-cyclohexyl ester (R)-2,3-dibutoxy-propyl ester

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Technology Process of Phosphoric acid (1S,2R,3R,4R,5R,6S)-2,5-bis-benzyloxy-3,4-bis-(bis-benzyloxy-phosphoryloxy)-6-fluoro-cyclohexyl ester (R)-2,3-dibutoxy-propyl ester

There total 12 articles about Phosphoric acid (1S,2R,3R,4R,5R,6S)-2,5-bis-benzyloxy-3,4-bis-(bis-benzyloxy-phosphoryloxy)-6-fluoro-cyclohexyl ester (R)-2,3-dibutoxy-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 208844-98-8
Phosphoric acid mono-((R)-2,3-dibutoxy-propyl) ester

: 208844-97-7
Phosphoric acid dibenzyl ester (1R,2S,3S,4R,5R,6R)-2,5-bis-benzyloxy-6-(bis-benzyloxy-phosphoryloxy)-4-fluoro-3-hydroxy-cyclohexyl ester

: 208844-99-9
Phosphoric acid (1S,2R,3R,4R,5R,6S)-2,5-bis-benzyloxy-3,4-bis-(bis-benzyloxy-phosphoryloxy)-6-fluoro-cyclohexyl ester (R)-2,3-dibutoxy-propyl ester

Guidance literature:: With pyridine; Triphenylsilyl chloride; at 22 ℃; for 3h;
DOI:10.1016/S0960-894X(98)00172-3

Reference yield:

: 366495-87-6
(S)-2,3-Dibutoxy-propan-1-ol

: 208844-99-9
Phosphoric acid (1S,2R,3R,4R,5R,6S)-2,5-bis-benzyloxy-3,4-bis-(bis-benzyloxy-phosphoryloxy)-6-fluoro-cyclohexyl ester (R)-2,3-dibutoxy-propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1H-tetrazole, m-CPBA / CH₂Cl₂ / -40 °C

2: H₂ / Pd/C / 2327.2 Torr

3: 70 percent / TPSCl, Py / 3 h / 22 °C

With pyridine; 1H-tetrazole; Triphenylsilyl chloride; hydrogen; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In dichloromethane;
DOI:10.1016/S0960-894X(98)00172-3

Reference yield:

: 366495-86-5
((R)-2,3-Dibutoxy-propoxymethyl)-benzene

: 208844-99-9
Phosphoric acid (1S,2R,3R,4R,5R,6S)-2,5-bis-benzyloxy-3,4-bis-(bis-benzyloxy-phosphoryloxy)-6-fluoro-cyclohexyl ester (R)-2,3-dibutoxy-propyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: H₂ / Pd/C / 2327.2 Torr

2: 1H-tetrazole, m-CPBA / CH₂Cl₂ / -40 °C

3: H₂ / Pd/C / 2327.2 Torr

4: 70 percent / TPSCl, Py / 3 h / 22 °C

With pyridine; 1H-tetrazole; Triphenylsilyl chloride; hydrogen; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In dichloromethane;
DOI:10.1016/S0960-894X(98)00172-3