4-pentylcyclohexanenitrile

Base Information

Chemical Name:4-pentylcyclohexanenitrile
CAS No.:70997-11-4
Molecular Formula:C₁₂H₂₁N
Molecular Weight:179.305
Hs Code.:

Synonyms:4-pentylcyclohexanenitrile

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Chemical Property of 4-pentylcyclohexanenitrile

Chemical Property:

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Technology Process of 4-pentylcyclohexanenitrile

There total 1 articles about 4-pentylcyclohexanenitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 70997-11-4
4-pentylcyclohexanenitrile

Guidance literature:: 4-Pentyl-cyclohexancarbonsaeureamid, Dehydratisierung;

Reference yield:

: 70997-11-4
4-pentylcyclohexanenitrile

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: C₁₃H₂₁NO

Guidance literature:: 4-pentylcyclohexanenitrile; With n-butyllithium; diisopropylamine; In tetrahydrofuran; at -85 - -78 ℃; for 2h; Inert atmosphere;

N,N-dimethyl-formamide; In tetrahydrofuran; at -85 - 20 ℃; for 2h; Inert atmosphere;

Reference yield:

: 70997-11-4
4-pentylcyclohexanenitrile

: 2-(4-Pentyl-cyclohexyl)-6-propyl-1,2,3,4-tetrahydro-naphthalene

Guidance literature:: Multi-step reaction with 8 steps

1: diethyl ether

2: Zn / benzene / 70 - 75 °C

3: 70percent aq. HClO₄ / acetic acid / 50 °C / vacuum

4: H₂ / 10percent Pd/C / ethanol / Ambient temperature

5: NaOH / H₂O; CH₂Cl₂; methanol

6: SOCl₂ / dimethylformamide; toluene / Ambient temperature

7: AlCl₃ / CH₂Cl₂ / -50 °C

8: H₂ / 10percent Pd/C / ethanol; dioxane / Ambient temperature

With sodium hydroxide; aluminium trichloride; thionyl chloride; perchloric acid; hydrogen; zinc; palladium on activated charcoal; In 1,4-dioxane; methanol; diethyl ether; ethanol; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; toluene; benzene;
DOI:10.1002/hlca.19820650423