2-hydroxy-N,N,N-trimethylethanaminium 4-((2-((2-methoxyphenyl)carbamoyl)phenyl)thio)benzoate

Base Information

Chemical Name:2-hydroxy-N,N,N-trimethylethanaminium 4-((2-((2-methoxyphenyl)carbamoyl)phenyl)thio)benzoate
CAS No.:1379464-72-8
Molecular Formula:C₅H₁₄NO*C₂₁H₁₆NO₄S
Molecular Weight:482.601
Hs Code.:

Synonyms:2-hydroxy-N,N,N-trimethylethanaminium 4-((2-((2-methoxyphenyl)carbamoyl)phenyl)thio)benzoate

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Chemical Property of 2-hydroxy-N,N,N-trimethylethanaminium 4-((2-((2-methoxyphenyl)carbamoyl)phenyl)thio)benzoate

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Technology Process of 2-hydroxy-N,N,N-trimethylethanaminium 4-((2-((2-methoxyphenyl)carbamoyl)phenyl)thio)benzoate

There total 5 articles about 2-hydroxy-N,N,N-trimethylethanaminium 4-((2-((2-methoxyphenyl)carbamoyl)phenyl)thio)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1379464-70-6
4-((2-((2-methoxyphenyl)carbamoyl)phenyl)thio)benzoic acid

: 123-41-1
cholin hydroxide

: 1379464-72-8
2-hydroxy-N,N,N-trimethylethanaminium 4-((2-((2-methoxyphenyl)carbamoyl)phenyl)thio)benzoate

Guidance literature:: In methanol; ethyl acetate; at 50 - 60 ℃;
DOI:10.1021/ml300037k

Reference yield:

: 1379464-67-1
2-((4-(methoxycarbonyl)phenyl)thio)benzoic acid

: 1379464-72-8
2-hydroxy-N,N,N-trimethylethanaminium 4-((2-((2-methoxyphenyl)carbamoyl)phenyl)thio)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / N,N-dimethyl-formamide; benzene / 80 °C

1.2: 6 h / 80 °C

2.1: trimethyltin(IV) hydroxide / 1,2-dichloro-ethane / 6 h / 80 °C

3.1: methanol; ethyl acetate / 50 - 60 °C

With thionyl chloride; trimethyltin(IV) hydroxide; In methanol; ethyl acetate; 1,2-dichloro-ethane; N,N-dimethyl-formamide; benzene;
DOI:10.1021/ml300037k

Reference yield:

: 1379464-68-2
methyl 4-((2-((2-methoxyphenyl)carbamoyl)phenyl)thio)benzoate

: 1379464-72-8
2-hydroxy-N,N,N-trimethylethanaminium 4-((2-((2-methoxyphenyl)carbamoyl)phenyl)thio)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: trimethyltin(IV) hydroxide / 1,2-dichloro-ethane / 6 h / 80 °C

2: methanol; ethyl acetate / 50 - 60 °C

With trimethyltin(IV) hydroxide; In methanol; ethyl acetate; 1,2-dichloro-ethane;
DOI:10.1021/ml300037k