Technology Process of C31H34O6S
There total 9 articles about C31H34O6S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tris(dimethylamino)sulfonium trimethylsilyldifluoride; oxygen; phosphorous acid trimethyl ester;
In
acetonitrile;
at -37 ℃;
for 0.833333h;
DOI:10.1021/jo00243a001
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 2.) 2,3-dichloro-5,6-dicyano-1,4-benzoquinone (DDQ) / 1.) toluene, 134 deg C, 72 h, 2.) dioxane, 70 deg C, 15.5 h
2: 95 percent / tris(dimethylamino)sulfonium difluorotrimethylsilicate (TASF), (MeO)3P, O2 / acetonitrile / 0.83 h / -37 °C
With
tris(dimethylamino)sulfonium trimethylsilyldifluoride; oxygen; 2,3-dicyano-5,6-dichloro-p-benzoquinone; phosphorous acid trimethyl ester;
In
acetonitrile;
DOI:10.1021/jo00243a001
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 71 percent / Jones reagent / CH2Cl2; diethyl ether / 0.5 h / 0 °C
2: 2.) 2,3-dichloro-5,6-dicyano-1,4-benzoquinone (DDQ) / 1.) toluene, 134 deg C, 72 h, 2.) dioxane, 70 deg C, 15.5 h
3: 95 percent / tris(dimethylamino)sulfonium difluorotrimethylsilicate (TASF), (MeO)3P, O2 / acetonitrile / 0.83 h / -37 °C
With
jones reagent; tris(dimethylamino)sulfonium trimethylsilyldifluoride; oxygen; 2,3-dicyano-5,6-dichloro-p-benzoquinone; phosphorous acid trimethyl ester;
In
diethyl ether; dichloromethane; acetonitrile;
DOI:10.1021/jo00243a001