4-(4-amino-2-methylpyrimidin-5-yl)methyl-6-(2-hydroxyethyl)-2-(2-methoxyphenyl)-5-methyl-2,3-dihydro-4H-1,4-thiazin-3-one

Base Information

• Chemical Name: 4-(4-amino-2-methylpyrimidin-5-yl)methyl-6-(2-hydroxyethyl)-2-(2-methoxyphenyl)-5-methyl-2,3-dihydro-4H-1,4-thiazin-3-one
• CAS No.: 7692-38-8
• Molecular Formula: C₂₀H₂₄N₄O₃S
• Molecular Weight: 400.502

Synonyms:4-(4-amino-2-methylpyrimidin-5-yl)methyl-6-(2-hydroxyethyl)-2-(2-methoxyphenyl)-5-methyl-2,3-dihydro-4H-1,4-thiazin-3-one

Chemical Property of 4-(4-amino-2-methylpyrimidin-5-yl)methyl-6-(2-hydroxyethyl)-2-(2-methoxyphenyl)-5-methyl-2,3-dihydro-4H-1,4-thiazin-3-one

Chemical Property:

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Technology Process of 4-(4-amino-2-methylpyrimidin-5-yl)methyl-6-(2-hydroxyethyl)-2-(2-methoxyphenyl)-5-methyl-2,3-dihydro-4H-1,4-thiazin-3-one

There total 1 articles about 4-(4-amino-2-methylpyrimidin-5-yl)methyl-6-(2-hydroxyethyl)-2-(2-methoxyphenyl)-5-methyl-2,3-dihydro-4H-1,4-thiazin-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 4-(4-amino-2-methylpyrimidin-5-yl)methyl-6-(2-hydroxyethyl)-2-(2-methoxyphenyl)-5-methyl-2,3-dihydro-4H-1,4-thiazin-3-one (7692-38-8)

Guidance literature:

Thiamin,Diaethyl-2-methoxybenzoylphosphonat;

Reference yield: 7.0%

4-(4-amino-2-methylpyrimidin-5-yl)methyl-6-(2-hydroxyethyl)-2-(2-methoxyphenyl)-5-methyl-2,3-dihydro-4H-1,4-thiazin-3-one (7692-38-8) → 2-Methoxybenzoic acid (579-75-9) + 2-oxido-1,2-oxathiolane-3-spiro-3'-<1'-(4-amino-2-methylpyrimidin-5-yl)methyl-4'-hydroxy-2'-methylene-4'-(2-methoxyphenyl)-tetrahydropyrrol-5'-one> (74982-37-9) + N-<(4-amino-2-methylpyrimidin-5-yl)methyl>-N-<1-(2-oxido-1,2-oxathiolan-3-ylidene)ethyl>-(2-methoxyphenyl)oxalamide (66666-34-0)

Guidance literature:

With dihydrogen peroxide; In acetic acid; for 56h; Ambient temperature;

DOI:10.1248/cpb.28.769

Reference yield:

4-(4-amino-2-methylpyrimidin-5-yl)methyl-6-(2-hydroxyethyl)-2-(2-methoxyphenyl)-5-methyl-2,3-dihydro-4H-1,4-thiazin-3-one (7692-38-8) → 6-(4-amino-2-methyl-pyrimidin-5-ylmethyl)-4-hydroxy-4-(2-methoxy-phenyl)-6a-methyl-hexahydro-furo[2,3-b]pyrrol-5-one (66666-38-4) + 1-(4-amino-2-methylpyrimidin-5-yl)methyl-4-hydroxy-3-(2-hydroxyethyl)-4-(2-methoxyphenyl)-2-methyl-Δ2-pyrrolin-5-one (66666-37-3)

Guidance literature:

With dihydrogen peroxide; In acetic acid;

DOI:10.1248/cpb.26.722

Downstream raw materials:

6-(4-amino-2-methyl-pyrimidin-5-ylmethyl)-4-hydroxy-4-(2-methoxy-phenyl)-6a-methyl-hexahydro-furo[2,3-b]pyrrol-5-one

1-(4-amino-2-methylpyrimidin-5-yl)methyl-4-hydroxy-3-(2-hydroxyethyl)-4-(2-methoxyphenyl)-2-methyl-Δ²-pyrrolin-5-one

2-Methoxybenzoic acid

2-oxido-1,2-oxathiolane-3-spiro-3'-<1'-(4-amino-2-methylpyrimidin-5-yl)methyl-4'-hydroxy-2'-methylene-4'-(2-methoxyphenyl)-tetrahydropyrrol-5'-one>

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