Technology Process of C18H34O3Si
There total 8 articles about C18H34O3Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N,N,N,N,N-hexamethylphosphoric triamide / 3 h / -15 °C
2: diisobutylaluminium hydride / dichloromethane / 1 h / 0 °C
With
tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride;
In
N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane;
DOI:10.1016/j.tetlet.2011.12.015
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 0.25 h
2: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N,N,N,N,N-hexamethylphosphoric triamide / 3 h / -15 °C
3: diisobutylaluminium hydride / dichloromethane / 1 h / 0 °C
With
sodium tetrahydroborate; cerium(III) chloride heptahydrate; tetra-(n-butyl)ammonium iodide; sodium hydride; diisobutylaluminium hydride;
In
methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dichloromethane;
1: Luche reduction;
DOI:10.1016/j.tetlet.2011.12.015