(1R,4R)-1,7,7-trimethyl-2-(phenylamino)bicyclo[2.2.1]heptane-2-carbonitrile

Base Information

Chemical Name:(1R,4R)-1,7,7-trimethyl-2-(phenylamino)bicyclo[2.2.1]heptane-2-carbonitrile
CAS No.:911850-12-9
Molecular Formula:C₁₇H₂₂N₂
Molecular Weight:254.375
Hs Code.:

Synonyms:(1R,4R)-1,7,7-trimethyl-2-(phenylamino)bicyclo[2.2.1]heptane-2-carbonitrile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R,4R)-1,7,7-trimethyl-2-(phenylamino)bicyclo[2.2.1]heptane-2-carbonitrile

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Technology Process of (1R,4R)-1,7,7-trimethyl-2-(phenylamino)bicyclo[2.2.1]heptane-2-carbonitrile

There total 1 articles about (1R,4R)-1,7,7-trimethyl-2-(phenylamino)bicyclo[2.2.1]heptane-2-carbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 464-49-3,68546-28-1
(1R,4R)-1,7,7-trimethylbicyclo[2.2.1]heptan-2-one

: 143-33-9,25596-52-5
sodium cyanide

: 62-53-3
aniline

: 911850-12-9
(1R,4R)-1,7,7-trimethyl-2-(phenylamino)bicyclo[2.2.1]heptane-2-carbonitrile

Guidance literature:: In acetic acid; for 0.5h;
DOI:10.1002/jhet.5570430444

Reference yield: 95.0%

: 911850-12-9
(1R,4R)-1,7,7-trimethyl-2-(phenylamino)bicyclo[2.2.1]heptane-2-carbonitrile

: 28627-52-3
N-((1R,4R)-1,7,7-trimethylbicyclo[2.2.1]heptane-2-ylidene)benzenamine

Guidance literature:: With potassium hydroxide; In methanol; for 1.25h; Heating;
DOI:10.1002/jhet.5570430444

Reference yield:

: 911850-12-9
(1R,4R)-1,7,7-trimethyl-2-(phenylamino)bicyclo[2.2.1]heptane-2-carbonitrile

: 485319-27-5
(5S,8R)-3-bromo-3-butyl-8,9,9-trimethyl-1-phenyl-5,6,7,8-tetrahydro-5,8-methanoquinoline-2,4(1H,3H)-dione

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / potassium hydroxide / methanol / 1.25 h / Heating

2: 63 percent / 1.5 h / 240 - 250 °C

3: 68 percent / bromine / CHCl₃

With potassium hydroxide; bromine; In methanol; chloroform;
DOI:10.1002/jhet.5570430444