Technology Process of benzyl 3-cyclohexylideneprop-2-en-1-yl carbonate
There total 4 articles about benzyl 3-cyclohexylideneprop-2-en-1-yl carbonate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine; dmap;
In
dichloromethane;
at 0 - 20 ℃;
for 120h;
Inert atmosphere;
DOI:10.1002/chem.201103902
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / diethyl ether; hexane / 0.75 h / -78 °C / Inert atmosphere
1.2: -78 - 20 °C / Inert atmosphere
2.1: lithium aluminium tetrahydride / diethyl ether / 5 h / 0 - 20 °C / Inert atmosphere
3.1: pyridine; dmap / dichloromethane / 120 h / 0 - 20 °C / Inert atmosphere
With
pyridine; dmap; lithium aluminium tetrahydride; n-butyllithium;
In
diethyl ether; hexane; dichloromethane;
DOI:10.1002/chem.201103902
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: toluene-4-sulfonic acid / dichloromethane / 5 h / 0 °C / Inert atmosphere
2.1: n-butyllithium / diethyl ether; hexane / 0.75 h / -78 °C / Inert atmosphere
2.2: -78 - 20 °C / Inert atmosphere
3.1: lithium aluminium tetrahydride / diethyl ether / 5 h / 0 - 20 °C / Inert atmosphere
4.1: pyridine; dmap / dichloromethane / 120 h / 0 - 20 °C / Inert atmosphere
With
pyridine; dmap; lithium aluminium tetrahydride; n-butyllithium; toluene-4-sulfonic acid;
In
diethyl ether; hexane; dichloromethane;
DOI:10.1002/chem.201103902
