4-(3'-amino-4',5'-dimethoxyphenyl)-5-(4''-N,N-dimethylaminophenyl)oxazole

Base Information

Chemical Name:4-(3'-amino-4',5'-dimethoxyphenyl)-5-(4''-N,N-dimethylaminophenyl)oxazole
CAS No.:1245716-26-0
Molecular Formula:C₁₉H₂₁N₃O₃
Molecular Weight:339.394
Hs Code.:

Synonyms:4-(3'-amino-4',5'-dimethoxyphenyl)-5-(4''-N,N-dimethylaminophenyl)oxazole

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Chemical Property of 4-(3'-amino-4',5'-dimethoxyphenyl)-5-(4''-N,N-dimethylaminophenyl)oxazole

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Technology Process of 4-(3'-amino-4',5'-dimethoxyphenyl)-5-(4''-N,N-dimethylaminophenyl)oxazole

There total 3 articles about 4-(3'-amino-4',5'-dimethoxyphenyl)-5-(4''-N,N-dimethylaminophenyl)oxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1245716-20-4
4-(3',4'-dimethoxy-5'-nitrophenyl)-5-(4''-N,N-dimethylaminophenyl)oxazole

: 1245716-26-0
4-(3'-amino-4',5'-dimethoxyphenyl)-5-(4''-N,N-dimethylaminophenyl)oxazole

Guidance literature:: With 5% Pd(II)/C(eggshell); ammonium formate; In methanol; for 2h; Reflux;
DOI:10.1021/jm100345r

Reference yield:

: 1345961-99-0
3,4-dimethoxy-5-nitrophenyl(tosyl)methyl isocyanide

: 1245716-26-0
4-(3'-amino-4',5'-dimethoxyphenyl)-5-(4''-N,N-dimethylaminophenyl)oxazole

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / methanol; 1,2-dimethoxyethane / 2 h

2: ammonium formate / 5%-palladium/activated carbon / methanol / 2 h / Reflux

With ammonium formate; potassium carbonate; 5%-palladium/activated carbon; In methanol; 1,2-dimethoxyethane;

Reference yield:

: 1245716-03-3
N-[(toluene-4-sulfonyl)-(3,4-dimethoxy-5-nitrophenyl)methyl]formamide

: 1245716-26-0
4-(3'-amino-4',5'-dimethoxyphenyl)-5-(4''-N,N-dimethylaminophenyl)oxazole

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine; trichlorophosphate / 1,2-dimethoxyethane / -10 - -5 °C

2: potassium carbonate / methanol; 1,2-dimethoxyethane / 2 h

3: ammonium formate / 5%-palladium/activated carbon / methanol / 2 h / Reflux

With ammonium formate; potassium carbonate; triethylamine; trichlorophosphate; 5%-palladium/activated carbon; In methanol; 1,2-dimethoxyethane;