2,6-bis[p-(N,N-dimethylamino)phenyl]-4,8-dibromobenzo[1,2-d;4,5-d']bisoxazole

Base Information

Chemical Name:2,6-bis[p-(N,N-dimethylamino)phenyl]-4,8-dibromobenzo[1,2-d;4,5-d']bisoxazole
CAS No.:1350803-88-1
Molecular Formula:C₂₄H₂₀Br₂N₄O₂
Molecular Weight:556.256
Hs Code.:

Synonyms:2,6-bis[p-(N,N-dimethylamino)phenyl]-4,8-dibromobenzo[1,2-d;4,5-d']bisoxazole

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Chemical Property of 2,6-bis[p-(N,N-dimethylamino)phenyl]-4,8-dibromobenzo[1,2-d;4,5-d']bisoxazole

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Technology Process of 2,6-bis[p-(N,N-dimethylamino)phenyl]-4,8-dibromobenzo[1,2-d;4,5-d']bisoxazole

There total 1 articles about 2,6-bis[p-(N,N-dimethylamino)phenyl]-4,8-dibromobenzo[1,2-d;4,5-d']bisoxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 619-84-1
p-N,N-dimethylaminobenzoic acid

: 81534-82-9
3,6-diamino-2,5-dibromo-1,4-hydroquinone

: 1350803-88-1
2,6-bis[p-(N,N-dimethylamino)phenyl]-4,8-dibromobenzo[1,2-d;4,5-d']bisoxazole

Guidance literature:: p-N,N-dimethylaminobenzoic acid; 3,6-diamino-2,5-dibromo-1,4-hydroquinone; With phosphoric acid; at 160 ℃; for 24h;

With sodium hydroxide; In water;
DOI:10.1021/jo202107w

Reference yield: 72.0%

: 1350803-88-1
2,6-bis[p-(N,N-dimethylamino)phenyl]-4,8-dibromobenzo[1,2-d;4,5-d']bisoxazole

: 536-74-3
phenylacetylene

: 1350803-82-5
C₄₀H₃₀N₄O₂

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In acetonitrile; at 100 ℃; for 3h; Microwave irradiation;
DOI:10.1021/jo202107w

Reference yield: 61.0%

: 1350803-88-1
2,6-bis[p-(N,N-dimethylamino)phenyl]-4,8-dibromobenzo[1,2-d;4,5-d']bisoxazole

: 1066-54-2
trimethylsilylacetylene

: 1446406-44-5
C₃₄H₃₈N₄O₂Si₂

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine; In tetrahydrofuran; at 120 ℃; for 168h; Inert atmosphere; Sealed tube;
DOI:10.1021/ol401120a