({(2R,3S,5S)-1-(benzyloxy)-5-[(4-methoxybenzyl)oxy]-2,6-dimethylhept-6-en-3-yl}oxy)(tert-butyl)diphenylsilane

Base Information

• Chemical Name: ({(2R,3S,5S)-1-(benzyloxy)-5-[(4-methoxybenzyl)oxy]-2,6-dimethylhept-6-en-3-yl}oxy)(tert-butyl)diphenylsilane
• CAS No.: 1092368-90-5
• Molecular Formula: C₄₀H₅₀O₄Si
• Molecular Weight: 622.92

Synonyms:({(2R,3S,5S)-1-(benzyloxy)-5-[(4-methoxybenzyl)oxy]-2,6-dimethylhept-6-en-3-yl}oxy)(tert-butyl)diphenylsilane

Chemical Property of ({(2R,3S,5S)-1-(benzyloxy)-5-[(4-methoxybenzyl)oxy]-2,6-dimethylhept-6-en-3-yl}oxy)(tert-butyl)diphenylsilane

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Technology Process of ({(2R,3S,5S)-1-(benzyloxy)-5-[(4-methoxybenzyl)oxy]-2,6-dimethylhept-6-en-3-yl}oxy)(tert-butyl)diphenylsilane

There total 2 articles about ({(2R,3S,5S)-1-(benzyloxy)-5-[(4-methoxybenzyl)oxy]-2,6-dimethylhept-6-en-3-yl}oxy)(tert-butyl)diphenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

C47H58O7SSi (1092368-89-2) → ({(2R,3S,5S)-1-(benzyloxy)-5-[(4-methoxybenzyl)oxy]-2,6-dimethylhept-6-en-3-yl}oxy)(tert-butyl)diphenylsilane (1092368-90-5)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium iodide; In 1,2-dimethoxyethane; at 85 ℃; for 2.5h;

DOI:10.1055/s-2008-1078170

Reference yield: 80.0%

7-O-benzyl-5-O-[tert-butyl(diphenyl)silyl]-2,4,6-trideoxy-3-O-(4-methoxybenzyl)-2,6-dimethyl-1-O-[(4-methylphenyl)sulfonyl]-D-gluco-heptitol → ({(2R,3S,5S)-1-(benzyloxy)-5-[(4-methoxybenzyl)oxy]-2,6-dimethylhept-6-en-3-yl}oxy)(tert-butyl)diphenylsilane (1092368-90-5)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium iodide; In 1,2-dimethoxyethane; for 3h; Reflux; Inert atmosphere;

DOI:10.1055/s-0029-1216903

Reference yield: 85.0%

({(2R,3S,5S)-1-(benzyloxy)-5-[(4-methoxybenzyl)oxy]-2,6-dimethylhept-6-en-3-yl}oxy)(tert-butyl)diphenylsilane (1092368-90-5) → C39H48O5Si (1092368-91-6)

Guidance literature:

With 2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide; In tetrahydrofuran; water; at 20 ℃; for 4h;

DOI:10.1055/s-2008-1078170

upstream raw materials:

C₄₇H₅₈O₇SSi

Downstream raw materials:

C₃₉H₄₈O₅Si

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