2-O-(2-O-acetyl-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl chloride

Base Information

Chemical Name:2-O-(2-O-acetyl-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl chloride
CAS No.:172471-70-4
Molecular Formula:C₂₈H₃₃ClN₆O₇
Molecular Weight:601.059
Hs Code.:

Synonyms:2-O-(2-O-acetyl-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-O-(2-O-acetyl-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl chloride

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2-O-(2-O-acetyl-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl chloride

There total 1 articles about 2-O-(2-O-acetyl-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 172471-69-1
Acetic acid (2R,3S,4S,5R,6R)-5-azido-2-[(2S,3S,4S,5R,6R)-5-azido-4-benzyloxy-6-methyl-2-(2-trimethylsilanyl-ethoxy)-tetrahydro-pyran-3-yloxy]-4-benzyloxy-6-methyl-tetrahydro-pyran-3-yl ester

: 172471-70-4
2-O-(2-O-acetyl-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl chloride

Guidance literature:: With Dichloromethyl methyl ether; zinc(II) chloride; In dichloromethane; for 3h; Ambient temperature;
DOI:10.1016/0008-6215(96)00202-9

Reference yield: 95.0%

: 172471-70-4
2-O-(2-O-acetyl-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl chloride

: 172471-72-6
2-(trimethylsilyl)ethyl (4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1-> 2)-[(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1-> 2)]₂-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranoside

: 2-(trimethylsilyl)ethyl (2-O-acetyl-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1-> 2)-[(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1-> 2)]₄-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranoside

Guidance literature:: With 2,6-di-tert-butyl-4-methylpyridine; silver trifluoromethanesulfonate; In dichloromethane; for 1h;
DOI:10.1016/0008-6215(96)00202-9

Reference yield: 83.0%

: 172471-70-4
2-O-(2-O-acetyl-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl chloride

: 172471-71-5
2-(trimethylsilyl)ethyl 4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl-(1→2)-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranoside

: 2-(trimethylsilyl)ethyl (2-O-acetyl-4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1-> 2)-(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1-> 2)-(4-azido-3-O-benzyl-4,6-dideoxy-α-D-mannopyranosyl)-(1-> 2)-4-azido-3-O-benzyl-4,6-dideox...

Guidance literature:: With 2,6-di-tert-butyl-4-methylpyridine; silver trifluoromethanesulfonate; In dichloromethane; for 1h;
DOI:10.1016/0008-6215(96)00202-9