Diphenyl<1-(3-hydroxypropoxy)>essigsaeure-piperid-4'-yl-esterhydrochlorid

Base Information

Chemical Name:Diphenyl<1-(3-hydroxypropoxy)>essigsaeure-piperid-4'-yl-esterhydrochlorid
CAS No.:118108-68-2
Molecular Formula:C₂₂H₂₇NO₄*ClH
Molecular Weight:405.922
Hs Code.:

Synonyms:Diphenyl<1-(3-hydroxypropoxy)>essigsaeure-piperid-4'-yl-esterhydrochlorid

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Chemical Property of Diphenyl<1-(3-hydroxypropoxy)>essigsaeure-piperid-4'-yl-esterhydrochlorid

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Technology Process of Diphenyl<1-(3-hydroxypropoxy)>essigsaeure-piperid-4'-yl-esterhydrochlorid

There total 6 articles about Diphenyl<1-(3-hydroxypropoxy)>essigsaeure-piperid-4'-yl-esterhydrochlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 118108-67-1
Diphenyl<1-(3-hydroxypropoxy)>essigsaeure-(1'-benzylpiperid-4'-yl)esterhydrochlorid

: 118108-68-2
Diphenyl<1-(3-hydroxypropoxy)>essigsaeure-piperid-4'-yl-esterhydrochlorid

Guidance literature:: With hydrogen; nickel; In methanol; at 30 ℃; for 3h; under 735.5 Torr; Yield given;

Reference yield:

: 118108-61-5
1-benzylpiperidin-4-yl 2-hydroxy-2,2-diphenylacetate

: 118108-68-2
Diphenyl<1-(3-hydroxypropoxy)>essigsaeure-piperid-4'-yl-esterhydrochlorid

Guidance literature:: Multi-step reaction with 3 steps

1: 93 percent / H₂ / 10 percent Pd/C / methanol; acetic acid / 4 h / 30 °C

2: SOCl₂, DMF / chlorobenzene / 10 h / 90 - 95 °C

With thionyl chloride; hydrogen; N,N-dimethyl-formamide; palladium on activated charcoal; In methanol; acetic acid; chlorobenzene;

Reference yield:

: 76-89-1
methyl benzilate

: 118108-68-2
Diphenyl<1-(3-hydroxypropoxy)>essigsaeure-piperid-4'-yl-esterhydrochlorid

Guidance literature:: Multi-step reaction with 4 steps

1: 67.6 percent / 10 percent CH₃ONa / petroleum ether; methanol / 4.5 h / Heating

2: 93 percent / H₂ / 10 percent Pd/C / methanol; acetic acid / 4 h / 30 °C

3: SOCl₂, DMF / chlorobenzene / 10 h / 90 - 95 °C

With thionyl chloride; hydrogen; sodium methylate; N,N-dimethyl-formamide; palladium on activated charcoal; In methanol; acetic acid; chlorobenzene; Petroleum ether;