C₃₄H₅₇NO₄Si₂

Base Information

Chemical Name:C₃₄H₅₇NO₄Si₂
CAS No.:1438399-48-4
Molecular Formula:C₃₄H₅₇NO₄Si₂
Molecular Weight:600.002
Hs Code.:

C<sub>34</sub>H<sub>57</sub>NO<sub>4</sub>Si<sub>2</sub>

Synonyms:C₃₄H₅₇NO₄Si₂

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Chemical Property of C₃₄H₅₇NO₄Si₂

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Technology Process of C₃₄H₅₇NO₄Si₂

There total 3 articles about C₃₄H₅₇NO₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1438399-46-2
C₃₃H₅₃NO₄Si₂

: 69739-34-0
t-butyldimethylsiyl triflate

: 1438399-48-4
C₃₄H₅₇NO₄Si₂

Guidance literature:: C₃₃H₅₃NO₄Si₂; With copper(l) iodide; methyllithium; In tetrahydrofuran; diethyl ether; at 0 ℃; for 8h; Inert atmosphere;

t-butyldimethylsiyl triflate; With 2,6-dimethylpyridine; In dichloromethane; at 0 ℃; Inert atmosphere;
DOI:10.1002/chem.201201332

Reference yield:

: 1195779-19-1
C₃₀H₄₃NO₄SSi

: 1438399-48-4
C₃₄H₅₇NO₄Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: copper(l) iodide; methyllithium / tetrahydrofuran; diethyl ether / 8 h / 0 °C / Inert atmosphere

1.2: 0.5 h / 0 °C / Inert atmosphere

2.1: lithium triethylborohydride / tetrahydrofuran / 0.5 h / 0 - 25 °C / Inert atmosphere

3.1: [bis(acetoxy)iodo]benzene; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / 0.5 h / 0 °C

4.1: dichloromethane / 12 h / 25 °C / Inert atmosphere

5.1: copper(l) iodide; methyllithium / tetrahydrofuran; diethyl ether / 8 h / 0 °C / Inert atmosphere

5.2: 0 °C / Inert atmosphere

With copper(l) iodide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; methyllithium; lithium triethylborohydride; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1002/chem.201201332

Reference yield:

: 1438399-44-0
C₃₇H₆₁NO₄SSi₂

: 1438399-48-4
C₃₄H₅₇NO₄Si₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium triethylborohydride / tetrahydrofuran / 0.5 h / 0 - 25 °C / Inert atmosphere

2.1: [bis(acetoxy)iodo]benzene; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane / 0.5 h / 0 °C

3.1: dichloromethane / 12 h / 25 °C / Inert atmosphere

4.1: copper(l) iodide; methyllithium / tetrahydrofuran; diethyl ether / 8 h / 0 °C / Inert atmosphere

4.2: 0 °C / Inert atmosphere

With copper(l) iodide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; [bis(acetoxy)iodo]benzene; methyllithium; lithium triethylborohydride; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1002/chem.201201332