3-tert-Butyl-1-(diphenylphosphoryl)-5-phenyl-1H-1,2,4-diazaphosphol

Base Information

• Chemical Name: 3-tert-Butyl-1-(diphenylphosphoryl)-5-phenyl-1H-1,2,4-diazaphosphol
• CAS No.: 108592-93-4
• Molecular Formula: C₂₄H₂₄N₂OP₂
• Molecular Weight: 418.415
• Mol file: 108592-93-4.mol

Synonyms:3-tert-Butyl-1-(diphenylphosphoryl)-5-phenyl-1H-1,2,4-diazaphosphol

Chemical Property of 3-tert-Butyl-1-(diphenylphosphoryl)-5-phenyl-1H-1,2,4-diazaphosphol

Chemical Property:

Purity/Quality:

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Technology Process of 3-tert-Butyl-1-(diphenylphosphoryl)-5-phenyl-1H-1,2,4-diazaphosphol

There total 1 articles about 3-tert-Butyl-1-(diphenylphosphoryl)-5-phenyl-1H-1,2,4-diazaphosphol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2,2-dimethylpropylidynephosphine (78129-68-7) + (diphenylphosphinyl)phenyldiazomethane (17507-57-2) → 3-tert-Butyl-1-(diphenylphosphoryl)-5-phenyl-1H-1,2,4-diazaphosphol (108592-93-4)

Guidance literature:

In benzene; for 96h; Ambient temperature;

Reference yield: 81.0%

3-tert-Butyl-1-(diphenylphosphoryl)-5-phenyl-1H-1,2,4-diazaphosphol (108592-93-4) → 1H-3-phenyl-5-tert-butyl-1,2,4-diazaphosphole (108592-78-5)

Guidance literature:

With water; silica gel; In diethyl ether; for 5h;

upstream raw materials:

2,2-dimethylpropylidynephosphine

(diphenylphosphinyl)phenyldiazomethane

Downstream raw materials:

1H-3-phenyl-5-tert-butyl-1,2,4-diazaphosphole