6-O-acetyl-1',3',4',6'-tetra-O-benzyl-2-O-(4-methoxybenzyl)-4-O-((S)-2-methylbutyryl)sucrose

Base Information

Chemical Name:6-O-acetyl-1',3',4',6'-tetra-O-benzyl-2-O-(4-methoxybenzyl)-4-O-((S)-2-methylbutyryl)sucrose
CAS No.:178685-21-7
Molecular Formula:C₅₅H₆₄O₁₄
Molecular Weight:949.105
Hs Code.:

Synonyms:6-O-acetyl-1',3',4',6'-tetra-O-benzyl-2-O-(4-methoxybenzyl)-4-O-((S)-2-methylbutyryl)sucrose

Suppliers and Price of 6-O-acetyl-1',3',4',6'-tetra-O-benzyl-2-O-(4-methoxybenzyl)-4-O-((S)-2-methylbutyryl)sucrose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 6-O-acetyl-1',3',4',6'-tetra-O-benzyl-2-O-(4-methoxybenzyl)-4-O-((S)-2-methylbutyryl)sucrose

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 6-O-acetyl-1',3',4',6'-tetra-O-benzyl-2-O-(4-methoxybenzyl)-4-O-((S)-2-methylbutyryl)sucrose

There total 3 articles about 6-O-acetyl-1',3',4',6'-tetra-O-benzyl-2-O-(4-methoxybenzyl)-4-O-((S)-2-methylbutyryl)sucrose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1730-91-2
(S)-2-Methylbutyric acid

: 178685-21-7
6-O-acetyl-1',3',4',6'-tetra-O-benzyl-2-O-(4-methoxybenzyl)-4-O-((S)-2-methylbutyryl)sucrose

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / dicyclohexylcarbodiimide, 4-methylaminopyridine / CCl₄ / Ambient temperature

2: 1.) tris(triphenylphosphine)rhodium(I) chloride, 2.) HgBr₂ / 1.) toluene, EtOH, H₂O, reflux, 24 h, 2.) toluene, EtOH, H₂O, 16 h

With 4-(Methylamino)pyridine; Wilkinson's catalyst; dicyclohexyl-carbodiimide; mercury dibromide; In tetrachloromethane;
DOI:10.1016/0008-6215(96)00026-2

Reference yield:

: 100980-32-3
6-O-acetyl-3-O-allyl-1',3',4',6'-tetra-O-benzyl-2-O-(4-methoxybenzyl)sucrose

: 178685-21-7
6-O-acetyl-1',3',4',6'-tetra-O-benzyl-2-O-(4-methoxybenzyl)-4-O-((S)-2-methylbutyryl)sucrose

Guidance literature:: Multi-step reaction with 2 steps

1: 96 percent / dicyclohexylcarbodiimide, 4-methylaminopyridine / CCl₄ / Ambient temperature

2: 1.) tris(triphenylphosphine)rhodium(I) chloride, 2.) HgBr₂ / 1.) toluene, EtOH, H₂O, reflux, 24 h, 2.) toluene, EtOH, H₂O, 16 h

With 4-(Methylamino)pyridine; Wilkinson's catalyst; dicyclohexyl-carbodiimide; mercury dibromide; In tetrachloromethane;
DOI:10.1016/0008-6215(96)00026-2

Reference yield:

: 178685-20-6
6-O-acetyl-3-O-allyl-1',3',4',6'-tetra-O-benzyl-2-O-(4-methoxybenzyl)-4-O-((S)-2-methylbutyryl)sucrose

: 178685-21-7
6-O-acetyl-1',3',4',6'-tetra-O-benzyl-2-O-(4-methoxybenzyl)-4-O-((S)-2-methylbutyryl)sucrose

Guidance literature:: With Wilkinson's catalyst; mercury dibromide; Yield given. Multistep reaction; 1.) toluene, EtOH, H₂O, reflux, 24 h, 2.) toluene, EtOH, H₂O, 16 h;
DOI:10.1016/0008-6215(96)00026-2