Technology Process of C51H64O8
There total 9 articles about C51H64O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C19H22O5;
With
2,4,6-trichlorobenzoyl chloride; triethylamine;
In
toluene;
at 20 ℃;
for 2h;
C32H44O4;
With
dmap;
In
toluene;
at 50 ℃;
for 1h;
DOI:10.1021/jm300566h
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: water; toluene-4-sulfonic acid / tetrahydrofuran; water; acetonitrile / 2 h / 20 °C
2.1: mercury(II) perchlorate hexahydrate / dichloromethane; water; acetonitrile / 1 h / 4 °C
3.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 2 h / 20 °C
3.2: 1 h / 50 °C
With
mercury(II) perchlorate hexahydrate; 2,4,6-trichlorobenzoyl chloride; water; toluene-4-sulfonic acid; triethylamine;
In
tetrahydrofuran; dichloromethane; water; toluene; acetonitrile;
DOI:10.1021/jm300566h
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: mercury(II) perchlorate hexahydrate / dichloromethane; water; acetonitrile / 1 h / 4 °C
2.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 2 h / 20 °C
2.2: 1 h / 50 °C
With
mercury(II) perchlorate hexahydrate; 2,4,6-trichlorobenzoyl chloride; triethylamine;
In
dichloromethane; water; toluene; acetonitrile;
DOI:10.1021/jm300566h