isopropyl rac-1-(phenylsulfinyl)naphthalene-2-carboxylate

Base Information

Chemical Name:isopropyl rac-1-(phenylsulfinyl)naphthalene-2-carboxylate
CAS No.:264872-23-3
Molecular Formula:C₂₀H₁₈O₃S
Molecular Weight:338.427
Hs Code.:

Synonyms:isopropyl rac-1-(phenylsulfinyl)naphthalene-2-carboxylate

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Chemical Property of isopropyl rac-1-(phenylsulfinyl)naphthalene-2-carboxylate

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Technology Process of isopropyl rac-1-(phenylsulfinyl)naphthalene-2-carboxylate

There total 5 articles about isopropyl rac-1-(phenylsulfinyl)naphthalene-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 719278-26-9
isopropyl 1-(phenylsulfanyl)naphthalene-2-carboxylate

: 264872-23-3
isopropyl rac-1-(phenylsulfinyl)naphthalene-2-carboxylate

Guidance literature:: isopropyl 1-(phenylsulfanyl)naphthalene-2-carboxylate; With ethylene diamine tetraacetic acid tetrasodium salt; sodium hydrogencarbonate; acetone; In acetonitrile; at 4 - 8 ℃; for 2h;

With oxone; In acetonitrile; for 7h;
DOI:10.1016/j.jorganchem.2004.03.021

Reference yield:

: 20717-79-7
1-bromo-2-naphthoic acid

: 264872-23-3
isopropyl rac-1-(phenylsulfinyl)naphthalene-2-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: SOCl₂; pyridine / benzene / 18 h / 25 °C

1.2: 53 g / pyridine / CH₂Cl₂ / 1 h / 25 °C

2.1: sodium hydride / dimethylformamide / 0.25 h / 0 °C

2.2: 85 percent / dimethylformamide / 18 h / 70 °C

3.1: sodium EDTA; acetone; sodium hydrogen carbonate / acetonitrile / 2 h / 4 - 8 °C

3.2: 86 percent / OXONE(R) / acetonitrile / 7 h

With pyridine; thionyl chloride; ethylene diamine tetraacetic acid tetrasodium salt; sodium hydride; sodium hydrogencarbonate; acetone; In N,N-dimethyl-formamide; acetonitrile; benzene;
DOI:10.1016/j.jorganchem.2004.03.021

Reference yield:

: 719278-25-8
isopropyl 1-bromonaphthalene-2-carboxylate

: 264872-23-3
isopropyl rac-1-(phenylsulfinyl)naphthalene-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / dimethylformamide / 0.25 h / 0 °C

1.2: 85 percent / dimethylformamide / 18 h / 70 °C

2.1: sodium EDTA; acetone; sodium hydrogen carbonate / acetonitrile / 2 h / 4 - 8 °C

2.2: 86 percent / OXONE(R) / acetonitrile / 7 h

With ethylene diamine tetraacetic acid tetrasodium salt; sodium hydride; sodium hydrogencarbonate; acetone; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.jorganchem.2004.03.021