2-(3-methyl-4-(3-oxo-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3H-xanthen-9-yl)phenoxy)acetic acid

Base Information

Chemical Name:2-(3-methyl-4-(3-oxo-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3H-xanthen-9-yl)phenoxy)acetic acid
CAS No.:1219603-03-8
Molecular Formula:C₂₈H₂₇BO₇
Molecular Weight:486.329
Hs Code.:

Synonyms:2-(3-methyl-4-(3-oxo-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3H-xanthen-9-yl)phenoxy)acetic acid

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Chemical Property of 2-(3-methyl-4-(3-oxo-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3H-xanthen-9-yl)phenoxy)acetic acid

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Technology Process of 2-(3-methyl-4-(3-oxo-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3H-xanthen-9-yl)phenoxy)acetic acid

There total 1 articles about 2-(3-methyl-4-(3-oxo-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3H-xanthen-9-yl)phenoxy)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1219603-02-7
tert-butyl-2-(3-methyl-4-(3-oxo-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3H-xanthen-9-yl)phenoxy)acetate

: 1219603-03-8
2-(3-methyl-4-(3-oxo-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3H-xanthen-9-yl)phenoxy)acetic acid

Guidance literature:: With trifluoroacetic acid; In CH₂Cl₂; (N2); dropwise addn. of a soln. of boron compd. in CH2Cl2 to a mixt. of CH2Cl2/TFA, stirring for 4 h; evapn. in vac., flash column chromy. (silica gel, methanol/ CH2Cl2 1:10);
DOI:10.1021/ja100117u

Reference yield: 53.0%

: 913817-45-5
4-((4-(aminomethyl)benzyl)oxy)-6-chloropyrimidin-2-amine

: 1219603-03-8
2-(3-methyl-4-(3-oxo-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3H-xanthen-9-yl)phenoxy)acetic acid

: 1219603-05-0
N-(4-((2-amino-6-chloropyrimidin-4-yloxy)methyl)benzyl)-2-(3-methyl-4-(3-oxo-6-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-3H-xanthen-9-yl)phenoxy)acetamide

Guidance literature:: With N,N,N',N'-Me₄-O-(7-azabenzotriazol-1-yl)uroniumPF₆; diisopropylethylamine; In dimethylformamide; (N2); dissolving boron compd. in DMF, stirring at room temp. for 5 min, addn. of HATU, amino deriv., DIPEA, stirring at room temp. overnight; evapn. in vac., dissolving in 10%methanol in CH2Cl2, flash column chromy. (silica gel, methanol/CH2Cl2 1:10);
DOI:10.1021/ja100117u