(2S,3S)-2-(3,4-dichlorophenyl)3-(1,3-dioxo-1,3-dihydroisoindol-2-yl)-4-nitrobutyraldehyde

Base Information

Chemical Name:(2S,3S)-2-(3,4-dichlorophenyl)3-(1,3-dioxo-1,3-dihydroisoindol-2-yl)-4-nitrobutyraldehyde
CAS No.:1233691-99-0
Molecular Formula:C₁₈H₁₂Cl₂N₂O₅
Molecular Weight:407.21
Hs Code.:

Synonyms:(2S,3S)-2-(3,4-dichlorophenyl)3-(1,3-dioxo-1,3-dihydroisoindol-2-yl)-4-nitrobutyraldehyde

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Chemical Property of (2S,3S)-2-(3,4-dichlorophenyl)3-(1,3-dioxo-1,3-dihydroisoindol-2-yl)-4-nitrobutyraldehyde

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Technology Process of (2S,3S)-2-(3,4-dichlorophenyl)3-(1,3-dioxo-1,3-dihydroisoindol-2-yl)-4-nitrobutyraldehyde

There total 2 articles about (2S,3S)-2-(3,4-dichlorophenyl)3-(1,3-dioxo-1,3-dihydroisoindol-2-yl)-4-nitrobutyraldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1233692-08-4
β-phthalimidonitroethene

: 93467-56-2
2-(3',4'-dichlorophenyl)acetaldehyde

: 2-(3,4-dichlorophenyl)3-(1,3-dioxo-1,3-dihydro-isoindol-2-yl)-4-nitrobutyraldehyde

: 1233691-99-0
(2S,3S)-2-(3,4-dichlorophenyl)3-(1,3-dioxo-1,3-dihydroisoindol-2-yl)-4-nitrobutyraldehyde

Guidance literature:: With (R)-2-(diphenyl(trimethylsilyloxy)methyl)pyrrolidine; acetic acid; In acetonitrile; at 0 - 20 ℃; Overall yield = 98 %;

Reference yield:

: 1238305-33-3
(E)-2-(2-nitrovinyl)isoindoline-1,3-dione

: 93467-56-2
2-(3',4'-dichlorophenyl)acetaldehyde

: 1233691-99-0
(2S,3S)-2-(3,4-dichlorophenyl)3-(1,3-dioxo-1,3-dihydroisoindol-2-yl)-4-nitrobutyraldehyde

: 2-(3,4-dichlorophenyl)3-(1,3-dioxo-1,3-dihydroisoindol-2-yl)-4-nitrobutyraldehyde

: 2-(3,4-dichlorophenyl)3-(1,3-dioxo-1,3-dihydroisoindol-2-yl)-4-nitrobutyraldehyde

Guidance literature:: With acetic acid; In acetonitrile; at 0 ℃; for 6h; optical yield given as %ee; enantioselective reaction;
DOI:10.1002/anie.201001644