4-dodecyloxy-4'-(tetradecyloxy)benzyl

Base Information

• Chemical Name: 4-dodecyloxy-4'-(tetradecyloxy)benzyl
• CAS No.: 1219732-50-9
• Molecular Formula: C₄₀H₆₂O₄
• Molecular Weight: 606.93
• Mol file: 1219732-50-9.mol

Synonyms:4-dodecyloxy-4'-(tetradecyloxy)benzyl

Chemical Property of 4-dodecyloxy-4'-(tetradecyloxy)benzyl

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 4-dodecyloxy-4'-(tetradecyloxy)benzyl

There total 1 articles about 4-dodecyloxy-4'-(tetradecyloxy)benzyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

1-Bromotetradecane (112-71-0) + 4-dodecyloxy-4'-hydroxybenzil (1219732-61-2) → 4-dodecyloxy-4'-(tetradecyloxy)benzyl (1219732-50-9)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 90 ℃;

DOI:10.1039/b9nj00519f

Reference yield: 52.0%

tetraphosphorus decasulfide (15857-57-5) + nickel(II) chloride hexahydrate + 4-dodecyloxy-4'-(tetradecyloxy)benzyl (1219732-50-9) → bis[1-(4-dodecyloxyphenyl)-2-(4-tetradecyloxyphenyl)ethene-1,2-dithiolene]nickel (1219732-74-7)

Guidance literature:

With air; In dioxane; H₂O; mixt. of dialkoxybenzil and P4S10 in dioxane heated at 130°C under reflux for 5 h, hot mixture filtered, aq. soln. of NiCl2*6H2O added tofiltrate, mixt. heated under reflux for 2 h, cooled to room temp.; small amt. of H2O added, ppt. filtered off, repeated pptn. from CH2Cl2 by addn. of EtOH, column chromy. (silica gel, hexane/CH2Cl2); elem. anal.;

DOI:10.1039/b9nj00519f

Reference yield:

4-dodecyloxy-4'-(tetradecyloxy)benzyl (1219732-50-9) → C40H62O2S2

Guidance literature:

With tetraphosphorus decasulfide; In 1,4-dioxane; at 130 ℃; for 5h;

DOI:10.1039/b9nj00519f

upstream raw materials:

1-Bromotetradecane

4-dodecyloxy-4'-hydroxybenzil

Downstream raw materials:

bis[1-(4-dodecyloxyphenyl)-2-(4-tetradecyloxyphenyl)ethene-1,2-dithiolene]nickel

Refernces