2,4-Bis-diphenylvinylidene-1,3-bis-(tris-trimethylsilanyl-methyl)-[1,3]diarsetane

Base Information

Chemical Name:2,4-Bis-diphenylvinylidene-1,3-bis-(tris-trimethylsilanyl-methyl)-[1,3]diarsetane
CAS No.:132091-89-5
Molecular Formula:C₅₀H₇₄As₂Si₆
Molecular Weight:993.494
Hs Code.:

Synonyms:2,4-Bis-diphenylvinylidene-1,3-bis-(tris-trimethylsilanyl-methyl)-[1,3]diarsetane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,4-Bis-diphenylvinylidene-1,3-bis-(tris-trimethylsilanyl-methyl)-[1,3]diarsetane

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Technology Process of 2,4-Bis-diphenylvinylidene-1,3-bis-(tris-trimethylsilanyl-methyl)-[1,3]diarsetane

There total 6 articles about 2,4-Bis-diphenylvinylidene-1,3-bis-(tris-trimethylsilanyl-methyl)-[1,3]diarsetane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 132091-86-2
C₂₆H₄₁AsOSi₃

: 132091-89-5
2,4-Bis-diphenylvinylidene-1,3-bis-(tris-trimethylsilanyl-methyl)-[1,3]diarsetane

Guidance literature:: With tert.-butyl lithium; In tetrahydrofuran; at -97.5 ℃;
DOI:10.1016/S0040-4039(00)97056-4

Reference yield: 16.0%

: 132091-87-3
C₂₅H₃₈AsClSi₃

: 132091-89-5
2,4-Bis-diphenylvinylidene-1,3-bis-(tris-trimethylsilanyl-methyl)-[1,3]diarsetane

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; In diethyl ether; for 15h; Ambient temperature;
DOI:10.1016/S0040-4039(00)97056-4

Reference yield:

: 1068-69-5
Tris(trimethylsilyl)methane

: 132091-89-5
2,4-Bis-diphenylvinylidene-1,3-bis-(tris-trimethylsilanyl-methyl)-[1,3]diarsetane

Guidance literature:: Multi-step reaction with 4 steps

1: AsCl₃, n-BuLi

2: Heating

3: 63 percent / tetrahydrofuran / -78 °C

4: Kieselgel

With n-butyllithium; arsenic trichloride; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)97056-4