bis-tert-butyl 5-(7-chloro-1-(4-methoxybenzyl)-2-oxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-5-yl)pyrimidin-2-yl-bis-carbamate

Base Information

Chemical Name:bis-tert-butyl 5-(7-chloro-1-(4-methoxybenzyl)-2-oxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-5-yl)pyrimidin-2-yl-bis-carbamate
CAS No.:1251949-05-9
Molecular Formula:C₃₁H₃₄ClN₅O₆
Molecular Weight:608.094
Hs Code.:

Synonyms:bis-tert-butyl 5-(7-chloro-1-(4-methoxybenzyl)-2-oxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-5-yl)pyrimidin-2-yl-bis-carbamate

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Chemical Property of bis-tert-butyl 5-(7-chloro-1-(4-methoxybenzyl)-2-oxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-5-yl)pyrimidin-2-yl-bis-carbamate

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Technology Process of bis-tert-butyl 5-(7-chloro-1-(4-methoxybenzyl)-2-oxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-5-yl)pyrimidin-2-yl-bis-carbamate

There total 1 articles about bis-tert-butyl 5-(7-chloro-1-(4-methoxybenzyl)-2-oxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-5-yl)pyrimidin-2-yl-bis-carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1251949-04-8
tert-butyl 5-(7-chloro-1-(4-methoxybenzyl)-2-oxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-5-yl)pyrimidin-2-ylcarbamate

: 1251949-05-9
bis-tert-butyl 5-(7-chloro-1-(4-methoxybenzyl)-2-oxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-5-yl)pyrimidin-2-yl-bis-carbamate

Guidance literature:: With dmap; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

Reference yield:

: 1251949-05-9
bis-tert-butyl 5-(7-chloro-1-(4-methoxybenzyl)-2-oxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-5-yl)pyrimidin-2-yl-bis-carbamate

: 205816-93-9
4-(bromomethyl)-1,2-diethylbenzene

: 1251949-06-0
bis-tert-butyl 5-(7-chloro-3-(3,4-diethylbenzyl)-1-(4-methoxybenzyl)-2-oxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-5-yl)pyrimidin-2-yl(methyl)-bis-carbamate

Guidance literature:: bis-tert-butyl 5-(7-chloro-1-(4-methoxybenzyl)-2-oxo-2,3-dihydro-1H-benzo[e][1,4]diazepin-5-yl)pyrimidin-2-yl-bis-carbamate; With potassium tert-butylate; In tetrahydrofuran; at -78 ℃; for 0.166667h;

4-(bromomethyl)-1,2-diethylbenzene; In tetrahydrofuran; at -78 - 20 ℃;

With ammonium chloride; In tetrahydrofuran; water; ethyl acetate;