(tetratosyl-1',4',8',11'-tetraaza-1',4',8',11'-cyclotetradecyl-6')-4-butanol

Base Information

Chemical Name:(tetratosyl-1',4',8',11'-tetraaza-1',4',8',11'-cyclotetradecyl-6')-4-butanol
CAS No.:118467-59-7
Molecular Formula:C₄₂H₅₆N₄O₉S₄
Molecular Weight:889.192
Hs Code.:

Synonyms:(tetratosyl-1',4',8',11'-tetraaza-1',4',8',11'-cyclotetradecyl-6')-4-butanol

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Chemical Property of (tetratosyl-1',4',8',11'-tetraaza-1',4',8',11'-cyclotetradecyl-6')-4-butanol

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Technology Process of (tetratosyl-1',4',8',11'-tetraaza-1',4',8',11'-cyclotetradecyl-6')-4-butanol

There total 3 articles about (tetratosyl-1',4',8',11'-tetraaza-1',4',8',11'-cyclotetradecyl-6')-4-butanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 118467-56-4
(<(tetrahydro-3'',4'',5'',6''-2''H-pyranyl-2'')oxy>-4'-butyl)-6-tetratosyl-1,4,8,11-tetraaza-1,4,8,11-cyclotetradecane

: 118467-59-7
(tetratosyl-1',4',8',11'-tetraaza-1',4',8',11'-cyclotetradecyl-6')-4-butanol

Guidance literature:: With toluene-4-sulfonic acid; In 1,4-dioxane; for 2h; Yield given; Ambient temperature;
DOI:10.1002/hlca.19880710313

Reference yield:

: 111514-29-5
1,4,8,11-Tetrakis(toluene-p-sulphonyl)-1,4,8,11-tetraazaundecane

: 118467-59-7
(tetratosyl-1',4',8',11'-tetraaza-1',4',8',11'-cyclotetradecyl-6')-4-butanol

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / NaH / dimethylformamide / 2 h

2: TsOH / dioxane / 2 h / Ambient temperature

With sodium hydride; toluene-4-sulfonic acid; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19880710313

Reference yield:

: 118481-88-2
2-<4-(tetrahydropyran-2-yloxy)butyl>propane-1,3-diol di-p-toluenesulfonate

: 118467-59-7
(tetratosyl-1',4',8',11'-tetraaza-1',4',8',11'-cyclotetradecyl-6')-4-butanol

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / NaH / dimethylformamide / 2 h

2: TsOH / dioxane / 2 h / Ambient temperature

With sodium hydride; toluene-4-sulfonic acid; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19880710313