N,N-bis(4-methoxybenzyl)-3-nitrobenzenesulfonamide

Base Information

Chemical Name:N,N-bis(4-methoxybenzyl)-3-nitrobenzenesulfonamide
CAS No.:1294519-55-3
Molecular Formula:C₂₂H₂₂N₂O₆S
Molecular Weight:442.492
Hs Code.:

Synonyms:N,N-bis(4-methoxybenzyl)-3-nitrobenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-bis(4-methoxybenzyl)-3-nitrobenzenesulfonamide

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Technology Process of N,N-bis(4-methoxybenzyl)-3-nitrobenzenesulfonamide

There total 1 articles about N,N-bis(4-methoxybenzyl)-3-nitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 121-52-8
3-nitrophenylsulfonamide

: 824-94-2
p-methoxybenzyl chloride

: 1294519-55-3
N,N-bis(4-methoxybenzyl)-3-nitrobenzenesulfonamide

Guidance literature:: With potassium carbonate; sodium iodide; In butanone; at 80 ℃; for 16h;
DOI:10.1016/j.tetlet.2011.02.034

Reference yield: 100.0%

: 1294519-55-3
N,N-bis(4-methoxybenzyl)-3-nitrobenzenesulfonamide

: 1313595-44-6
3-amino-N,N-bis(4-methoxybenzyl)benzenesulfonamide

Guidance literature:: With platinum(IV) oxide; hydrogen; In ethanol; for 1h; under 760.051 Torr;
DOI:10.1016/j.tetlet.2011.02.034

Reference yield:

: 1294519-55-3
N,N-bis(4-methoxybenzyl)-3-nitrobenzenesulfonamide

: C₂₈H₂₈N₂O₄S

Guidance literature:: Multi-step reaction with 2 steps

1: platinum(IV) oxide; hydrogen / ethanol / 1 h / 760.05 Torr

2: palladium diacetate; caesium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene / 1,4-dioxane / 4 h / 85 °C / Inert atmosphere

With platinum(IV) oxide; hydrogen; palladium diacetate; caesium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; In 1,4-dioxane; ethanol; 2: Buchwald-Hartwig coupling;
DOI:10.1016/j.tetlet.2011.02.034