(E)-ethyl 2-(4-(cyclohexyl(hydroxyimino)methyl)-2-methylphenoxy)acetate

Base Information

Chemical Name:(E)-ethyl 2-(4-(cyclohexyl(hydroxyimino)methyl)-2-methylphenoxy)acetate
CAS No.:1268705-11-8
Molecular Formula:C₁₈H₂₅NO₄
Molecular Weight:319.401
Hs Code.:

Synonyms:(E)-ethyl 2-(4-(cyclohexyl(hydroxyimino)methyl)-2-methylphenoxy)acetate

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Chemical Property of (E)-ethyl 2-(4-(cyclohexyl(hydroxyimino)methyl)-2-methylphenoxy)acetate

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Technology Process of (E)-ethyl 2-(4-(cyclohexyl(hydroxyimino)methyl)-2-methylphenoxy)acetate

There total 3 articles about (E)-ethyl 2-(4-(cyclohexyl(hydroxyimino)methyl)-2-methylphenoxy)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1225386-33-3
ethyl 2-(4-(cyclohexanecarbonyl)-2-methylphenoxy)acetate

: 1268705-11-8
(E)-ethyl 2-(4-(cyclohexyl(hydroxyimino)methyl)-2-methylphenoxy)acetate

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In ethanol; water; for 1h; Reflux;
DOI:10.1016/j.bmc.2010.12.023

Reference yield:

: 18731-70-9
cyclohexyl-(4-hydroxy-3-methylphenyl)methanone

: 1268705-11-8
(E)-ethyl 2-(4-(cyclohexyl(hydroxyimino)methyl)-2-methylphenoxy)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 18 h / 60 °C

2: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 1 h / Reflux

With hydroxylamine hydrochloride; sodium acetate; potassium carbonate; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2010.12.023

Reference yield:

: 18731-58-3
cyclohexanecarboxylic 2-methylphenyl-ester

: 1268705-11-8
(E)-ethyl 2-(4-(cyclohexyl(hydroxyimino)methyl)-2-methylphenoxy)acetate

Guidance literature:: Multi-step reaction with 3 steps

1: aluminum (III) chloride / 2 h / 25 - 165 °C

2: potassium carbonate / N,N-dimethyl-formamide / 18 h / 60 °C

3: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 1 h / Reflux

With aluminum (III) chloride; hydroxylamine hydrochloride; sodium acetate; potassium carbonate; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2010.12.023