3-O-acetyl-2-azido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl nitrate

Base Information

Chemical Name:3-O-acetyl-2-azido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl nitrate
CAS No.:131326-57-3
Molecular Formula:C₁₅H₁₆N₄O₈
Molecular Weight:380.314
Hs Code.:

Synonyms:3-O-acetyl-2-azido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl nitrate

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Chemical Property of 3-O-acetyl-2-azido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl nitrate

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Technology Process of 3-O-acetyl-2-azido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl nitrate

There total 2 articles about 3-O-acetyl-2-azido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl nitrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 131432-51-4
3-O-acetyl-1,5-anhydro-4,6-O-benzylidene-2-deoxy-D-lyxo-hex-1-enitol

: 3-O-acetyl-2-azido-4,6-O-benzylidene-2-deoxy-α-D-talopyranosyl nitrate

: 131326-57-3
3-O-acetyl-2-azido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl nitrate

Guidance literature:: With sodium azide; ammonium cerium(IV) nitrate; In acetonitrile; at -20 ℃; for 4h;
DOI:10.1016/S0040-4020(01)87127-1

Reference yield:

: 124579-80-2,167074-37-5
1,5-anhydro-4,6-O-benzylidene-2-deoxy-D-lyxo-hex-1-enitol

: 131326-57-3
3-O-acetyl-2-azido-4,6-O-benzylidene-2-deoxy-α-D-galactopyranosyl nitrate

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / pyridine / 4-dimethylaminopyridine / 0.25 h / Ambient temperature

2: 44 percent / NaN₃, cerium(IV) ammonium nitrate / acetonitrile / 4 h / -20 °C

With pyridine; sodium azide; ammonium cerium(IV) nitrate; dmap; In acetonitrile;
DOI:10.1016/S0040-4020(01)87127-1