Technology Process of Benzenepropanoic acid, 4-(methoxycarbonyl)-, ethyl ester (9CI)
There total 4 articles about Benzenepropanoic acid, 4-(methoxycarbonyl)-, ethyl ester (9CI) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
[4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine]nickel(II) dichloride; tris-(trimethylsilyl)silane; [4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-N1,N1′]bis{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-κN]phenyl-κC}iridium(III) hexafluorophosphate; sodium carbonate;
In
1,2-dimethoxyethane;
at 20 ℃;
Glovebox;
Sealed tube;
Irradiation;
DOI:10.1021/acs.joc.1c01867
- Guidance literature:
-
Ethyl 3-bromopropionate;
With
indium; copper(l) iodide; lithium chloride;
In
tetrahydrofuran;
at 65 ℃;
for 12h;
methyl 4-iodobenzoate;
With
tetrakis(triphenylphosphine) palladium(0);
In
N,N-dimethyl acetamide;
at 90 ℃;
for 24h;
DOI:10.1039/c0cc05597b
- Guidance literature:
-
With
chloro-trimethyl-silane; tetrabutylammomium bromide;
In
N,N-dimethyl-formamide;
electroreduction at reactive Mg anode;
DOI:10.1016/S0040-4039(00)61132-2
