(S)-N-(2-(benzyloxy)-4-methoxybenzyl)-N-(1-hydroxy-4-methylpentan-2-yl)-4-methylbenzenesulfonamide

Base Information

Chemical Name:(S)-N-(2-(benzyloxy)-4-methoxybenzyl)-N-(1-hydroxy-4-methylpentan-2-yl)-4-methylbenzenesulfonamide
CAS No.:1208311-07-2
Molecular Formula:C₂₈H₃₅NO₅S
Molecular Weight:497.656
Hs Code.:

Synonyms:(S)-N-(2-(benzyloxy)-4-methoxybenzyl)-N-(1-hydroxy-4-methylpentan-2-yl)-4-methylbenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-N-(2-(benzyloxy)-4-methoxybenzyl)-N-(1-hydroxy-4-methylpentan-2-yl)-4-methylbenzenesulfonamide

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Technology Process of (S)-N-(2-(benzyloxy)-4-methoxybenzyl)-N-(1-hydroxy-4-methylpentan-2-yl)-4-methylbenzenesulfonamide

There total 9 articles about (S)-N-(2-(benzyloxy)-4-methoxybenzyl)-N-(1-hydroxy-4-methylpentan-2-yl)-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: C₂₉H₃₅NO₆S

: 1208311-07-2
(S)-N-(2-(benzyloxy)-4-methoxybenzyl)-N-(1-hydroxy-4-methylpentan-2-yl)-4-methylbenzenesulfonamide

Guidance literature:: C₂₉H₃₅NO₆S; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 1h;

With water; In tetrahydrofuran; ethyl acetate; at 0 ℃;
DOI:10.1016/j.bmcl.2009.10.126

Reference yield:

: C₂₉H₃₅NO₆S

: 1208311-07-2
(S)-N-(2-(benzyloxy)-4-methoxybenzyl)-N-(1-hydroxy-4-methylpentan-2-yl)-4-methylbenzenesulfonamide

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1016/j.bmcl.2013.10.013

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 1208311-07-2
(S)-N-(2-(benzyloxy)-4-methoxybenzyl)-N-(1-hydroxy-4-methylpentan-2-yl)-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / dichloromethane / 0.08 h / 0 °C / Inert atmosphere

1.2: 4 h / 0 - 25 °C / Inert atmosphere

2.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 12 h / 0 - 20 °C / Inert atmosphere

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

With lithium aluminium tetrahydride; triethylamine; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; 2.1: |Mitsunobu Displacement;
DOI:10.1016/j.bmcl.2013.10.013