13α-acetoxy-5α-cinnamoyloxy-2α-(methoxymethoxy)taxa-4(20),11-diene-9α,10β-diol

Base Information

Chemical Name:13α-acetoxy-5α-cinnamoyloxy-2α-(methoxymethoxy)taxa-4(20),11-diene-9α,10β-diol
CAS No.:477894-70-5
Molecular Formula:C₃₃H₄₄O₈
Molecular Weight:568.708
Hs Code.:

Synonyms:13α-acetoxy-5α-cinnamoyloxy-2α-(methoxymethoxy)taxa-4(20),11-diene-9α,10β-diol

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Chemical Property of 13α-acetoxy-5α-cinnamoyloxy-2α-(methoxymethoxy)taxa-4(20),11-diene-9α,10β-diol

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Technology Process of 13α-acetoxy-5α-cinnamoyloxy-2α-(methoxymethoxy)taxa-4(20),11-diene-9α,10β-diol

There total 3 articles about 13α-acetoxy-5α-cinnamoyloxy-2α-(methoxymethoxy)taxa-4(20),11-diene-9α,10β-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 477894-69-2
13α-acetoxy-5α-cinnamoyloxy-9α,10β-(dimethylmethylenedioxy)-2α-(methoxymethoxy)taxa-4(20),11-diene

: 477894-70-5
13α-acetoxy-5α-cinnamoyloxy-2α-(methoxymethoxy)taxa-4(20),11-diene-9α,10β-diol

Guidance literature:: With acetic acid; at 20 ℃; for 8h;
DOI:10.1021/np020240n

Reference yield:

: 477894-66-9
9α,10β-(dimethylmethylenedioxy)-2α-(methoxymethoxy)taxa-4(20),11-dien-5α,13α-diol

: 477894-70-5
13α-acetoxy-5α-cinnamoyloxy-2α-(methoxymethoxy)taxa-4(20),11-diene-9α,10β-diol

Guidance literature:: Multi-step reaction with 3 steps

1: 90 percent / pyridine; DMAP / 1 h / 20 °C

2: 99 percent / DMAP; pyridine / 16 h / 80 - 85 °C

3: 87 percent / aq. AcOH / 8 h / 20 °C

With pyridine; dmap; acetic acid;
DOI:10.1021/np020240n

Reference yield:

: 477894-68-1
13α-acetoxy-9α,10β-(dimethylmethylenedioxy)-2α-(methoxymethoxy)taxa-4(20),11-dien-5α-ol

: 477894-70-5
13α-acetoxy-5α-cinnamoyloxy-2α-(methoxymethoxy)taxa-4(20),11-diene-9α,10β-diol

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / DMAP; pyridine / 16 h / 80 - 85 °C

2: 87 percent / aq. AcOH / 8 h / 20 °C

With pyridine; dmap; acetic acid;
DOI:10.1021/np020240n