C₂₆H₄₀O₈

Base Information

Chemical Name:C₂₆H₄₀O₈
CAS No.:1520158-82-0
Molecular Formula:C₂₆H₄₀O₈
Molecular Weight:480.599
Hs Code.:

C<sub>26</sub>H<sub>40</sub>O<sub>8</sub>

Synonyms:C₂₆H₄₀O₈

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Chemical Property of C₂₆H₄₀O₈

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Technology Process of C₂₆H₄₀O₈

There total 5 articles about C₂₆H₄₀O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1520158-41-1
C₃₈H₇₀O₉Si₂

: 1520158-82-0
C₂₆H₄₀O₈

Guidance literature:: With ammonium bifluoride; In 1-methyl-pyrrolidin-2-one; N,N-dimethyl-formamide; at 20 - 100 ℃; for 36h;
DOI:10.1021/jo402167q

Reference yield:

: C₄₄H₇₄O₁₁SSi₂

: 1520158-82-0
C₂₆H₄₀O₈

Guidance literature:: Multi-step reaction with 2 steps

1: samarium diiodide / tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

2: ammonium bifluoride / N,N-dimethyl-formamide; 1-methyl-pyrrolidin-2-one / 36 h / 20 - 100 °C

With samarium diiodide; ammonium bifluoride; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; N,N-dimethyl-formamide;
DOI:10.1021/jo402167q

Reference yield:

: 148933-81-7
(2S,3S)-5-(tert-Butyl-dimethyl-silanyloxy)-3-(4-methoxy-benzyloxy)-2-methyl-pentanal

: 1520158-82-0
C₂₆H₄₀O₈

Guidance literature:: Multi-step reaction with 4 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 - 0 °C / Inert atmosphere

1.2: -78 °C / Inert atmosphere

2.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 0.5 h / 0 - 20 °C / Inert atmosphere

3.1: samarium diiodide / tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

4.1: ammonium bifluoride / N,N-dimethyl-formamide; 1-methyl-pyrrolidin-2-one / 36 h / 20 - 100 °C

With n-butyllithium; samarium diiodide; ammonium bifluoride; sodium hydrogencarbonate; Dess-Martin periodane; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo402167q