3-methoxy-4aβ,4b,5,6,7,8,10,10aβ-octahydro-4bβ,8,8-trimethyl-1,4-phenanthrenedione

Base Information

• Chemical Name: 3-methoxy-4aβ,4b,5,6,7,8,10,10aβ-octahydro-4bβ,8,8-trimethyl-1,4-phenanthrenedione
• CAS No.: 123151-54-2
• Molecular Formula: C₁₈H₂₄O₃
• Molecular Weight: 288.387

Synonyms:3-methoxy-4aβ,4b,5,6,7,8,10,10aβ-octahydro-4bβ,8,8-trimethyl-1,4-phenanthrenedione

Chemical Property of 3-methoxy-4aβ,4b,5,6,7,8,10,10aβ-octahydro-4bβ,8,8-trimethyl-1,4-phenanthrenedione

Chemical Property:

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Technology Process of 3-methoxy-4aβ,4b,5,6,7,8,10,10aβ-octahydro-4bβ,8,8-trimethyl-1,4-phenanthrenedione

There total 2 articles about 3-methoxy-4aβ,4b,5,6,7,8,10,10aβ-octahydro-4bβ,8,8-trimethyl-1,4-phenanthrenedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

1,3,3-trimethyl-2-vinylcyclohexene (5293-90-3) + 2-methoxy-1,4-benzoquinone (2880-58-2) → (4aR,4bS,10aR)-3-Methoxy-4b,8,8-trimethyl-4a,4b,5,6,7,8,10,10a-octahydro-phenanthrene-1,4-dione (123151-57-5) + 3-methoxy-4aβ,4b,5,6,7,8,10,10aβ-octahydro-4bβ,8,8-trimethyl-1,4-phenanthrenedione (123151-54-2)

Guidance literature:

In dichloromethane; for 336h; under 9000720 Torr; Title compound not separated from byproducts; Ambient temperature;

DOI:10.1021/jo00285a018

Reference yield: 80.0%

1,3,3-trimethyl-2-vinylcyclohexene (5293-90-3) + 2-methoxy-1,4-benzoquinone (2880-58-2) → 3-methoxy-4aβ,4b,5,6,7,8,10,10aβ-octahydro-4bβ,8,8-trimethyl-1,4-phenanthrenedione (123151-54-2)

Guidance literature:

In dichloromethane; for 336h; under 5250420 Torr;

DOI:10.1016/S0040-4039(00)96704-2

upstream raw materials:

1,3,3-trimethyl-2-vinylcyclohexene

2-methoxy-1,4-benzoquinone

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