O-{2-Azido-2-deoxy-O-[3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl-(1->3)]-O-[3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl-(1->6)]-α-D-galactopyranosyl}-N^α-(fluoren-9-ylmethoxycarbonyl)-L-threonine ...

Base Information

• Chemical Name: O-{2-Azido-2-deoxy-O-[3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl-(1->3)]-O-[3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl-(1->6)]-α-D-galactopyranosyl}-N^α-(fluoren-9-ylmethoxycarbonyl)-L-threonine ...
• CAS No.: 178447-06-8
• Molecular Formula: C₅₉H₅₇F₅N₆O₂₇S₄
• Molecular Weight: 1505.38

Synonyms:O-{2-Azido-2-deoxy-O-[3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl-(1->3)]-O-[3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl-(1->6)]-α-D-galactopyranosyl}-N^α-(fluoren-9-ylmethoxycarbonyl)-L-threonine ...

Chemical Property of O-{2-Azido-2-deoxy-O-[3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl-(1->3)]-O-[3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl-(1->6)]-α-D-galactopyranosyl}-N^α-(fluoren-9-ylmethoxycarbonyl)-L-threonine ...

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Technology Process of O-{2-Azido-2-deoxy-O-[3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl-(1->3)]-O-[3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl-(1->6)]-α-D-galactopyranosyl}-N^α-(fluoren-9-ylmethoxycarbonyl)-L-threonine ...

There total 1 articles about O-{2-Azido-2-deoxy-O-[3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl-(1->3)]-O-[3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl-(1->6)]-α-D-galactopyranosyl}-N^α-(fluoren-9-ylmethoxycarbonyl)-L-threonine ... which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

O-(3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl) trichloroacetimidate (162894-83-9) + C45H42F5N5O18S2 (178447-05-7) → O-{2-Azido-2-deoxy-O-[3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl-(1->3)]-O-[3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl-(1->6)]-α-D-galactopyranosyl}-Nα-(fluoren-9-ylmethoxycarbonyl)-L-threonine ... (178447-06-8)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; 3 A molecular sieve; In dichloromethane; at -30 ℃; for 0.5h;

DOI:10.1039/p19960000985

Reference yield: 61.0%

acetic anhydride (108-24-7) + O-{2-Azido-2-deoxy-O-[3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl-(1->3)]-O-[3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl-(1->6)]-α-D-galactopyranosyl}-Nα-(fluoren-9-ylmethoxycarbonyl)-L-threonine ... (178447-06-8) → O-{2-Acetamido-[2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->3)]-O-[2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl-(1->6)]-2-deoxy-α-D-galactopyranosyl}-Nα-(fluoren-9-ylmethoxycarbonyl)-L-threonine pentafluorophenyl ...

Guidance literature:

With copper(II) sulfate; acetic acid; zinc; In tetrahydrofuran; for 6h;

DOI:10.1039/p19960000985

Reference yield:

Fmoc-Lys(tert-butoxycarbonyl) (71989-26-9) + Fmoc-Gly-OPfp (86060-85-7) + N-(9-fluorenylmethoxycarbonyl)-L-leucine pentafluorophenyl ester (86060-88-0) + O-{2-Azido-2-deoxy-O-[3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl-(1->3)]-O-[3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl-(1->6)]-α-D-galactopyranosyl}-Nα-(fluoren-9-ylmethoxycarbonyl)-L-threonine ... (178447-06-8) → C74H122N14O30

Guidance literature:

With Macrosorb SPR 250 resin; Yield given. Multistep reaction;

DOI:10.1039/a606725e

upstream raw materials:

O-(3,4,6-tri-O-acetyl-2-deoxy-2-dithiasuccinimido-β-D-glucopyranosyl) trichloroacetimidate

C₄₅H₄₂F₅N₅O₁₈S₂

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