Methyl-[(E)-3-(1-p-tolyl-1H-[1,2,3]triazol-4-yl)-prop-2-en-(Z)-ylidene]-amine

Base Information

Chemical Name:Methyl-[(E)-3-(1-p-tolyl-1H-[1,2,3]triazol-4-yl)-prop-2-en-(Z)-ylidene]-amine
CAS No.:76621-25-5
Molecular Formula:C₁₃H₁₄N₄
Molecular Weight:226.281
Hs Code.:

Synonyms:Methyl-[(E)-3-(1-p-tolyl-1H-[1,2,3]triazol-4-yl)-prop-2-en-(Z)-ylidene]-amine

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Chemical Property of Methyl-[(E)-3-(1-p-tolyl-1H-[1,2,3]triazol-4-yl)-prop-2-en-(Z)-ylidene]-amine

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Technology Process of Methyl-[(E)-3-(1-p-tolyl-1H-[1,2,3]triazol-4-yl)-prop-2-en-(Z)-ylidene]-amine

There total 4 articles about Methyl-[(E)-3-(1-p-tolyl-1H-[1,2,3]triazol-4-yl)-prop-2-en-(Z)-ylidene]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 76621-20-0
C₁₃H₁₅N₄⁽¹⁺⁾*I^(1-)

: 76621-25-5
Methyl-[(E)-3-(1-p-tolyl-1H-[1,2,3]triazol-4-yl)-prop-2-en-(Z)-ylidene]-amine

Guidance literature:: With sodium hydroxide; In dichloromethane; water; for 24h; Ambient temperature;
DOI:10.1248/cpb.28.2083

Reference yield:

: 462-08-8
pyridin-3-ylamine

: 76621-25-5
Methyl-[(E)-3-(1-p-tolyl-1H-[1,2,3]triazol-4-yl)-prop-2-en-(Z)-ylidene]-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium nitrate, hydrochloric acid; 2.) sodium acetate / 1.) H₂O, 10-15 deg C, 1.5 h; 2.) H₂O, EtOH, 3 h, RT

2: 57 percent / ethanol / 3 h / Heating

3: 73 percent / NaOH / H₂O; CH₂Cl₂ / 24 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; sodium nitrate; sodium acetate; In ethanol; dichloromethane; water;
DOI:10.1248/cpb.28.2083

Reference yield:

: 106-49-0,12221-03-3
p-toluidine

: 76621-25-5
Methyl-[(E)-3-(1-p-tolyl-1H-[1,2,3]triazol-4-yl)-prop-2-en-(Z)-ylidene]-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium nitrate, hydrochloric acid; 2.) sodium acetate / 1.) H₂O, 10-15 deg C, 1.5 h; 2.) H₂O, EtOH, 3 h, RT

2: 57 percent / ethanol / 3 h / Heating

3: 73 percent / NaOH / H₂O; CH₂Cl₂ / 24 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; sodium nitrate; sodium acetate; In ethanol; dichloromethane; water;
DOI:10.1248/cpb.28.2083