Technology Process of 1-(4-methoxybenzyl)-4,6-bis(2,4,6-trimethoxyphenyl)-1,6-dihydropyridin-2(3H)-one
There total 4 articles about 1-(4-methoxybenzyl)-4,6-bis(2,4,6-trimethoxyphenyl)-1,6-dihydropyridin-2(3H)-one which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
silver (II) carbonate; palladium diacetate; propionic acid; triphenylphosphine;
In
N,N-dimethyl-formamide;
at 80 ℃;
for 24h;
DOI:10.1021/ol303497q
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: tetra-(n-butyl)ammonium iodide; potassium carbonate / acetone / 12 h
2.1: Super-Hydride? / toluene; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere
2.2: 2 h / 20 °C / Inert atmosphere
3.1: palladium diacetate; silver (II) carbonate; triphenylphosphine; propionic acid / N,N-dimethyl-formamide / 24 h / 80 °C
With
silver (II) carbonate; palladium diacetate; tetra-(n-butyl)ammonium iodide; potassium carbonate; propionic acid; triphenylphosphine;
In
tetrahydrofuran; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1021/ol303497q
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: Super-Hydride? / toluene; tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere
1.2: 2 h / 20 °C / Inert atmosphere
2.1: palladium diacetate; silver (II) carbonate; triphenylphosphine; propionic acid / N,N-dimethyl-formamide / 24 h / 80 °C
With
silver (II) carbonate; palladium diacetate; propionic acid; triphenylphosphine;
In
tetrahydrofuran; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol303497q
