5,8-benzyloxycarbonylimino-5,6,7,8-tetradeoxy-1,2-O-isopropylidene-α-D-allo-octose

Base Information

Chemical Name:5,8-benzyloxycarbonylimino-5,6,7,8-tetradeoxy-1,2-O-isopropylidene-α-D-allo-octose
CAS No.:144733-17-5
Molecular Formula:C₁₉H₂₅NO₆
Molecular Weight:363.411
Hs Code.:

Synonyms:5,8-benzyloxycarbonylimino-5,6,7,8-tetradeoxy-1,2-O-isopropylidene-α-D-allo-octose

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Chemical Property of 5,8-benzyloxycarbonylimino-5,6,7,8-tetradeoxy-1,2-O-isopropylidene-α-D-allo-octose

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Technology Process of 5,8-benzyloxycarbonylimino-5,6,7,8-tetradeoxy-1,2-O-isopropylidene-α-D-allo-octose

There total 1 articles about 5,8-benzyloxycarbonylimino-5,6,7,8-tetradeoxy-1,2-O-isopropylidene-α-D-allo-octose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 144691-15-6
5,8-benzyloxycarbonylimino-5,6,7,8-tetradeoxy-1,2-O-isopropylidene-α-D-octofuranosid-3-ulose-hydrate

: 144733-17-5
5,8-benzyloxycarbonylimino-5,6,7,8-tetradeoxy-1,2-O-isopropylidene-α-D-allo-octose

Guidance literature:: With sodium tetrahydroborate; In ethanol; for 2h; Ambient temperature;
DOI:10.1016/S0040-4020(01)86601-1

Reference yield:

: 144733-17-5
5,8-benzyloxycarbonylimino-5,6,7,8-tetradeoxy-1,2-O-isopropylidene-α-D-allo-octose

: 115438-57-8,115438-58-9
(R)-2-((2R,3S,4R)-3,4,5-Trihydroxy-tetrahydro-furan-2-yl)-pyrrolidine-1-carboxylic acid benzyl ester

Guidance literature:: With Amberlite IR-120(H+)resin; In water; at 45 ℃; for 3h;
DOI:10.1016/S0040-4020(01)86601-1

Reference yield:

: 144733-17-5
5,8-benzyloxycarbonylimino-5,6,7,8-tetradeoxy-1,2-O-isopropylidene-α-D-allo-octose

: (R)-2-((2R,3R,4S)-3-Fluoro-4,5-dihydroxy-tetrahydro-furan-2-yl)-pyrrolidine-1-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / CH₂Cl₂ / 0.33 h

2: tris-(dimethylamino)-sulfonium-difluoromethylsilicate (TASF) / CH₂Cl₂ / 1 h

3: Amberlite IR-120(H+)resin / H₂O / 3 h / 45 °C

With pyridine; Amberlite IR-120(H+)resin; tris(dimethylamino)sulfonium trimethylsilyldifluoride; In dichloromethane; water;
DOI:10.1016/S0040-4020(01)86601-1