pentafluorophenyl indirubin-5-carboxylate

Base Information

• Chemical Name: pentafluorophenyl indirubin-5-carboxylate
• CAS No.: 1238056-80-8
• Molecular Formula: C₂₃H₉F₅N₂O₄
• Molecular Weight: 472.327

Synonyms:pentafluorophenyl indirubin-5-carboxylate

Chemical Property of pentafluorophenyl indirubin-5-carboxylate

Chemical Property:

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Technology Process of pentafluorophenyl indirubin-5-carboxylate

There total 1 articles about pentafluorophenyl indirubin-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

pentafluorophenyl trifloroacetate (14533-84-7) + indirubin-5-carboxylic acid (1238056-78-4) → pentafluorophenyl indirubin-5-carboxylate (1238056-80-8)

Guidance literature:

With pyridine; dmap; In N,N-dimethyl-formamide; at 20 ℃; for 4h; Inert atmosphere;

DOI:10.1016/j.bmc.2010.04.066

Reference yield: 92.0%

4-(4-Methyl-piperazino)-anilin (16153-81-4) + pentafluorophenyl indirubin-5-carboxylate (1238056-80-8) → 5-{N-[4-(4-methylpiperazino)phenyl]aminocarbonyl}indirubin (1238056-87-5)

Guidance literature:

With dmap; In 1,4-dioxane; Inert atmosphere; Reflux;

DOI:10.1016/j.bmc.2010.04.066

Reference yield: 14.7%

pentafluorophenyl indirubin-5-carboxylate (1238056-80-8) + 4-amino-N,N-dimethylaniline (99-98-9) → 5-[N-(4-dimethylaminophenyl)aminocarbonyl]indirubin (1238056-93-3)

Guidance literature:

With dmap; In 1,4-dioxane; Inert atmosphere; Reflux;

DOI:10.1016/j.bmc.2010.04.066

upstream raw materials:

pentafluorophenyl trifloroacetate

indirubin-5-carboxylic acid

Downstream raw materials:

5-{N-[4-(4-methylpiperazino)phenyl]aminocarbonyl}indirubin

5-[N-(4-dimethylaminophenyl)aminocarbonyl]indirubin

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