cis-(1R,2S,4S)-N-[(1'-diphenylphosphinyl-(3'S)-3'-(2,6-dichlorophenyl)-(2'S)-2'-aziridinyl)carbonyl]bornane-10,2-sultam

Base Information

Chemical Name:cis-(1R,2S,4S)-N-[(1'-diphenylphosphinyl-(3'S)-3'-(2,6-dichlorophenyl)-(2'S)-2'-aziridinyl)carbonyl]bornane-10,2-sultam
CAS No.:887004-20-8
Molecular Formula:C₃₁H₃₁Cl₂N₂O₄PS
Molecular Weight:629.544
Hs Code.:

Synonyms:cis-(1R,2S,4S)-N-[(1'-diphenylphosphinyl-(3'S)-3'-(2,6-dichlorophenyl)-(2'S)-2'-aziridinyl)carbonyl]bornane-10,2-sultam

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Chemical Property of cis-(1R,2S,4S)-N-[(1'-diphenylphosphinyl-(3'S)-3'-(2,6-dichlorophenyl)-(2'S)-2'-aziridinyl)carbonyl]bornane-10,2-sultam

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Technology Process of cis-(1R,2S,4S)-N-[(1'-diphenylphosphinyl-(3'S)-3'-(2,6-dichlorophenyl)-(2'S)-2'-aziridinyl)carbonyl]bornane-10,2-sultam

There total 1 articles about cis-(1R,2S,4S)-N-[(1'-diphenylphosphinyl-(3'S)-3'-(2,6-dichlorophenyl)-(2'S)-2'-aziridinyl)carbonyl]bornane-10,2-sultam which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108448-77-7,124224-04-0
(+)-camphorsultam

: 887004-20-8
cis-(1R,2S,4S)-N-[(1'-diphenylphosphinyl-(3'S)-3'-(2,6-dichlorophenyl)-(2'S)-2'-aziridinyl)carbonyl]bornane-10,2-sultam

Guidance literature:: Multi-step reaction with 2 steps

1.1: 77 percent / n-BuLi / tetrahydrofuran; hexane / -78 °C

2.1: LiHMDS / tetrahydrofuran / 0.5 h / -78 °C

2.2: 87 percent / tetrahydrofuran / -78 °C

With n-butyllithium; lithium hexamethyldisilazane; In tetrahydrofuran; hexane; 2.2: Darzens reaction;
DOI:10.1016/j.tet.2006.01.068