N,N-dimethyl-4-(4-oxo-1-phenyl-1,3,8-triazaspiro[4.5]dec-8-yl)-2,2-diphenylbutyramide

Base Information

Chemical Name:N,N-dimethyl-4-(4-oxo-1-phenyl-1,3,8-triazaspiro[4.5]dec-8-yl)-2,2-diphenylbutyramide
CAS No.:630425-64-8
Molecular Formula:C₃₁H₃₆N₄O₂
Molecular Weight:496.652
Hs Code.:

Synonyms:N,N-dimethyl-4-(4-oxo-1-phenyl-1,3,8-triazaspiro[4.5]dec-8-yl)-2,2-diphenylbutyramide

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Chemical Property of N,N-dimethyl-4-(4-oxo-1-phenyl-1,3,8-triazaspiro[4.5]dec-8-yl)-2,2-diphenylbutyramide

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Technology Process of N,N-dimethyl-4-(4-oxo-1-phenyl-1,3,8-triazaspiro[4.5]dec-8-yl)-2,2-diphenylbutyramide

There total 2 articles about N,N-dimethyl-4-(4-oxo-1-phenyl-1,3,8-triazaspiro[4.5]dec-8-yl)-2,2-diphenylbutyramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 37743-18-3
N-(dihydro-3,3-diphenyl-2(3H)-furanylidene)-N-methylmethanaminium bromide

: 1021-25-6
1-Phenyl-1,3,8-triaza-spiro[4.5]decan-4-one

: 630425-64-8
N,N-dimethyl-4-(4-oxo-1-phenyl-1,3,8-triazaspiro[4.5]dec-8-yl)-2,2-diphenylbutyramide

Guidance literature:: With sodium carbonate; In DMF (N,N-dimethyl-formamide); at 80 ℃; for 1.5h;

Reference yield:

: 37742-98-6
4-Bromo-2,2-diphenylbutyric acid

: 630425-64-8
N,N-dimethyl-4-(4-oxo-1-phenyl-1,3,8-triazaspiro[4.5]dec-8-yl)-2,2-diphenylbutyramide

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride; N,N-dimethyl-formamide / chloroform / 4 h / Heating / reflux

2: sodium carbonate / tetrahydrofuran; water; toluene / 12 h

3: sodium carbonate / DMF (N,N-dimethyl-formamide) / 1.5 h / 80 °C

With thionyl chloride; sodium carbonate; N,N-dimethyl-formamide; In tetrahydrofuran; DMF (N,N-dimethyl-formamide); chloroform; water; toluene;

Reference yield: 71.0%

: 630425-64-8
N,N-dimethyl-4-(4-oxo-1-phenyl-1,3,8-triazaspiro[4.5]dec-8-yl)-2,2-diphenylbutyramide

: 539-74-2
Ethyl 3-bromopropionate

: 630425-65-9
3-[8-(3-dimethylcarbamoyl-3,3-diphenylpropyl)-4-oxo-1-phenyl-1,3,8-triazaspiro[4.5]dec-3-yl]propionic acid ethyl ester

Guidance literature:: N,N-dimethyl-4-(4-oxo-1-phenyl-1,3,8-triazaspiro[4.5]dec-8-yl)-2,2-diphenylbutyramide; With sodium hydride; In DMF (N,N-dimethyl-formamide); for 0.0333333h;

Ethyl 3-bromopropionate; In DMF (N,N-dimethyl-formamide); for 12h;