4-Benzyloxy-3-[2,4-bis-benzyloxy-6-(3-oxo-pentyl)-benzoyl]-6-methoxy-2-pentyl-benzoic acid methyl ester

Base Information

Chemical Name:4-Benzyloxy-3-[2,4-bis-benzyloxy-6-(3-oxo-pentyl)-benzoyl]-6-methoxy-2-pentyl-benzoic acid methyl ester
CAS No.:122849-77-8
Molecular Formula:C₄₇H₅₀O₈
Molecular Weight:742.909
Hs Code.:

Synonyms:4-Benzyloxy-3-[2,4-bis-benzyloxy-6-(3-oxo-pentyl)-benzoyl]-6-methoxy-2-pentyl-benzoic acid methyl ester

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Chemical Property of 4-Benzyloxy-3-[2,4-bis-benzyloxy-6-(3-oxo-pentyl)-benzoyl]-6-methoxy-2-pentyl-benzoic acid methyl ester

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Technology Process of 4-Benzyloxy-3-[2,4-bis-benzyloxy-6-(3-oxo-pentyl)-benzoyl]-6-methoxy-2-pentyl-benzoic acid methyl ester

There total 14 articles about 4-Benzyloxy-3-[2,4-bis-benzyloxy-6-(3-oxo-pentyl)-benzoyl]-6-methoxy-2-pentyl-benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 122849-75-6
5-<3,5-bis(benzyloxyphenyl)>pentan-3-one

: 78135-68-9
6-benzyloxy-4-methoxy-3-methoxycarbonyl-2-pentylbenzoic acid

: 122849-77-8
4-Benzyloxy-3-[2,4-bis-benzyloxy-6-(3-oxo-pentyl)-benzoyl]-6-methoxy-2-pentyl-benzoic acid methyl ester

Guidance literature:: With trifluoroacetic anhydride; In nitromethane; at 0 ℃; for 1.5h;

Reference yield:

: 24131-31-5
3,5-dibenzyloxybenzyl alcohol

: 122849-77-8
4-Benzyloxy-3-[2,4-bis-benzyloxy-6-(3-oxo-pentyl)-benzoyl]-6-methoxy-2-pentyl-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 9 steps

1: 95 percent / thionyl chloride, pyridine / CH₂Cl₂ / 3 h / Ambient temperature

2: 88 percent / dimethylformamide / 7 h / Ambient temperature

3: 91 percent / 30percent aq. sodium hydroxide / methanol / 72 h / Heating

4: 95 percent / potassium carbonate / acetone / 3 h / Heating

5: 95 percent / lithium aluminium hydride / diethyl ether / 2 h / Heating

6: 85 percent / pyridine / CHCl₃ / 3 h / 0 °C

7: 94 percent / 1,2-dimethoxyethane / dimethylsulfoxide / 18 h / Ambient temperature

8: 81 percent / ether / benzene / 1 h / Ambient temperature; aq. hydrochloric acid, ethyl acetate, 16 h

9: 98 percent / trifluoroacetic anhydride, / nitromethane / 1.5 h / 0 °C

With pyridine; sodium hydroxide; lithium aluminium tetrahydride; 1,2-dimethoxyethane; thionyl chloride; diethyl ether; potassium carbonate; trifluoroacetic anhydride; In methanol; diethyl ether; nitromethane; dichloromethane; chloroform; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; benzene;

Reference yield:

: 2732-96-9
3,5-dibenzyloxyphenylacetic acid

: 122849-77-8
4-Benzyloxy-3-[2,4-bis-benzyloxy-6-(3-oxo-pentyl)-benzoyl]-6-methoxy-2-pentyl-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 95 percent / potassium carbonate / acetone / 3 h / Heating

2: 95 percent / lithium aluminium hydride / diethyl ether / 2 h / Heating

3: 85 percent / pyridine / CHCl₃ / 3 h / 0 °C

4: 94 percent / 1,2-dimethoxyethane / dimethylsulfoxide / 18 h / Ambient temperature

5: 81 percent / ether / benzene / 1 h / Ambient temperature; aq. hydrochloric acid, ethyl acetate, 16 h

6: 98 percent / trifluoroacetic anhydride, / nitromethane / 1.5 h / 0 °C

With pyridine; lithium aluminium tetrahydride; 1,2-dimethoxyethane; diethyl ether; potassium carbonate; trifluoroacetic anhydride; In diethyl ether; nitromethane; chloroform; dimethyl sulfoxide; acetone; benzene;