(2E,4S)-2,2,5,5-tetramethyl-3-(2-methyl-1-oxo-2-butenyl)-4-phenylmethyloxazolidine

Base Information

Chemical Name:(2E,4S)-2,2,5,5-tetramethyl-3-(2-methyl-1-oxo-2-butenyl)-4-phenylmethyloxazolidine
CAS No.:265643-04-7
Molecular Formula:C₁₉H₂₇NO₂
Molecular Weight:301.429
Hs Code.:

Synonyms:(2E,4S)-2,2,5,5-tetramethyl-3-(2-methyl-1-oxo-2-butenyl)-4-phenylmethyloxazolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2E,4S)-2,2,5,5-tetramethyl-3-(2-methyl-1-oxo-2-butenyl)-4-phenylmethyloxazolidine

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Technology Process of (2E,4S)-2,2,5,5-tetramethyl-3-(2-methyl-1-oxo-2-butenyl)-4-phenylmethyloxazolidine

There total 1 articles about (2E,4S)-2,2,5,5-tetramethyl-3-(2-methyl-1-oxo-2-butenyl)-4-phenylmethyloxazolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 35660-94-7
(E)-2-methylbut-2-enoyl chloride

: 144899-42-3
(4S)-2,2,5,5-tetramethyl-4-phenylmethyloxazolidine

: 265643-04-7
(2E,4S)-2,2,5,5-tetramethyl-3-(2-methyl-1-oxo-2-butenyl)-4-phenylmethyloxazolidine

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/ol990405s

Reference yield:

: 265643-04-7
(2E,4S)-2,2,5,5-tetramethyl-3-(2-methyl-1-oxo-2-butenyl)-4-phenylmethyloxazolidine

: [S-(2R,3S)]-2,2,5,5-tetramethyl-3-[(2,3-dimethyloxiranyl)carbonyl]-4-phenylmethyloxazolidine

: [S-(2S,3R)]-2,2,5,5-tetramethyl-3-[(2,3-dimethyloxiranyl)carbonyl]-4-phenylmethyloxazolidine

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 24h; Title compound not separated from byproducts.;
DOI:10.1021/ol990405s

Reference yield:

: 265643-04-7
(2E,4S)-2,2,5,5-tetramethyl-3-(2-methyl-1-oxo-2-butenyl)-4-phenylmethyloxazolidine

: 3-(3-hydroxy-2-methylidene-1-oxobutyl)-2,2,5,5-tetramethyl-4-phenylmethyloxazolidine

Guidance literature:: (2E,4S)-2,2,5,5-tetramethyl-3-(2-methyl-1-oxo-2-butenyl)-4-phenylmethyloxazolidine; With oxygen; 5,15,10,20-tetraphenylporphyrin; In tetrachloromethane; at 0 ℃; for 48h; Irradiation;

With triphenylphosphine; In dichloromethane; at 0 ℃; for 0.25h;
DOI:10.1002/ejoc.200500077