4-(2-glyceryl)butyric acid-1-(2,4-dioxo-5,5-diphenyl-3-imidazolidinyl)methyl ester

Base Information

Chemical Name:4-(2-glyceryl)butyric acid-1-(2,4-dioxo-5,5-diphenyl-3-imidazolidinyl)methyl ester
CAS No.:155758-68-2
Molecular Formula:C₂₃H₂₆N₂O₇
Molecular Weight:442.469
Hs Code.:

Synonyms:4-(2-glyceryl)butyric acid-1-(2,4-dioxo-5,5-diphenyl-3-imidazolidinyl)methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(2-glyceryl)butyric acid-1-(2,4-dioxo-5,5-diphenyl-3-imidazolidinyl)methyl ester

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Technology Process of 4-(2-glyceryl)butyric acid-1-(2,4-dioxo-5,5-diphenyl-3-imidazolidinyl)methyl ester

There total 6 articles about 4-(2-glyceryl)butyric acid-1-(2,4-dioxo-5,5-diphenyl-3-imidazolidinyl)methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 155758-69-3
4-(1,3-dimyristoyl-2-glyceryl)butyric acid-1-(2,4-dioxo-5,5-diphenyl-3-imidazolidinyl)-methyl ester

: 57-41-0
phenythoin

: 155758-68-2
4-(2-glyceryl)butyric acid-1-(2,4-dioxo-5,5-diphenyl-3-imidazolidinyl)methyl ester

Guidance literature:: Product distribution; porcine pancreatic lipase;
DOI:10.1002/ardp.19943270512

Reference yield:

: 103024-90-4
1,3-di-O-benzyl-2-O-(2-hydroxyethyl)glycerol

: 155758-68-2
4-(2-glyceryl)butyric acid-1-(2,4-dioxo-5,5-diphenyl-3-imidazolidinyl)methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / CH₂Cl₂ / 0 °C

3: (COCl)2

4: 1.) Et₃N, 2.) H₂ / 2.) 10percent Pd/C / 1.) CH₂Cl₂, 0 deg C, 2 h, 2.) CH₂Cl₂, MeOH

With oxalyl dichloride; hydrogen; triethylamine; palladium on activated charcoal; In dichloromethane;
DOI:10.1002/ardp.19943270512

Reference yield:

: 155758-66-0
1,3-dibenzyl-2-glycerylacetic acid ethyl ester

: 155758-68-2
4-(2-glyceryl)butyric acid-1-(2,4-dioxo-5,5-diphenyl-3-imidazolidinyl)methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / LiAlH₄ / diethyl ether / 1 h / Ambient temperature

2: Et₃N / CH₂Cl₂ / 0 °C

4: (COCl)2

5: 1.) Et₃N, 2.) H₂ / 2.) 10percent Pd/C / 1.) CH₂Cl₂, 0 deg C, 2 h, 2.) CH₂Cl₂, MeOH

With lithium aluminium tetrahydride; oxalyl dichloride; hydrogen; triethylamine; palladium on activated charcoal; In diethyl ether; dichloromethane;
DOI:10.1002/ardp.19943270512