Z-L-Thz-O-Me

Base Information

Chemical Name:Z-L-Thz-O-Me
CAS No.:95716-08-8
Molecular Formula:C₂₁H₂₆N₂O₆S
Molecular Weight:434.513
Hs Code.:

Synonyms:Z-L-Thz-O-Me

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Z-L-Thz-O-Me

Chemical Property:

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Technology Process of Z-L-Thz-O-Me

There total 9 articles about Z-L-Thz-O-Me which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 92506-79-1,95782-97-1,95783-00-9,107032-93-9,107032-94-0
(S)-2-((S)-1-Benzyloxycarbonylamino-3-tert-butoxycarbonyl-propyl)-thiazolidine-4-carboxylic acid methyl ester

: 95716-08-8
Z-L-Thz-O-Me

Guidance literature:: With pyridine; manganese(IV) oxide; In benzene; at 55 ℃; for 4h;
DOI:10.1021/jo00383a014

Reference yield: 50.0%

: 92506-79-1,95782-97-1,95783-00-9,107032-93-9,107032-94-0
(R)-2-((S)-1-Benzyloxycarbonylamino-3-tert-butoxycarbonyl-propyl)-thiazolidine-4-carboxylic acid methyl ester

: 95716-08-8,106930-63-6
Z-L-(glu(OBu^t))Thz-OMe

Guidance literature:: With manganese(IV) oxide; benzene; at 60 ℃;
DOI:10.1016/S0040-4039(01)81589-6

Reference yield:

: 63648-73-7
N-benzyloxycarbonyl-D-glutamic acid

: 95716-08-8
Z-L-Thz-O-Me

Guidance literature:: Multi-step reaction with 5 steps

1: methanesulfonic acid / CH₂Cl₂ / 30 h / Ambient temperature

2: LiCl, NaBH₄ / tetrahydrofuran; ethanol / Ambient temperature

3: (CH₃)2SO, pyridine*SO₃ / CH₂Cl₂; triethylamine / 0.17 h / 10 - 20 °C

4: benzene / Ambient temperature

5: 50 percent / MnO₂, pyridine / benzene / 4 h / 55 °C

With pyridine; manganese(IV) oxide; sodium tetrahydroborate; methanesulfonic acid; sulfur trioxide pyridine complex; dimethyl sulfoxide; lithium chloride; In tetrahydrofuran; ethanol; dichloromethane; triethylamine; benzene;
DOI:10.1021/jo00383a014