2-(2-bromo-5-nitrophenoxy)-N-(2-chloro-4-fluorophenyl)-2-methylpropionamide

Base Information

• Chemical Name: 2-(2-bromo-5-nitrophenoxy)-N-(2-chloro-4-fluorophenyl)-2-methylpropionamide
• CAS No.: 945969-63-1
• Molecular Formula: C₁₆H₁₃BrClFN₂O₄
• Molecular Weight: 431.646

Synonyms:2-(2-bromo-5-nitrophenoxy)-N-(2-chloro-4-fluorophenyl)-2-methylpropionamide

Chemical Property of 2-(2-bromo-5-nitrophenoxy)-N-(2-chloro-4-fluorophenyl)-2-methylpropionamide

Chemical Property:

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Technology Process of 2-(2-bromo-5-nitrophenoxy)-N-(2-chloro-4-fluorophenyl)-2-methylpropionamide

There total 1 articles about 2-(2-bromo-5-nitrophenoxy)-N-(2-chloro-4-fluorophenyl)-2-methylpropionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethyl 2-(2-bromo-5-nitrophenoxy)-2-methylpropionate (945969-62-0) + 2-chloro-4-fluoroaniline (2106-02-7) → 2-(2-bromo-5-nitrophenoxy)-N-(2-chloro-4-fluorophenyl)-2-methylpropionamide (945969-63-1)

Guidance literature:

trimethylaluminum; In dichloromethane; toluene; at 20 ℃; for 1.5h;

Reference yield:

2-(2-bromo-5-nitrophenoxy)-N-(2-chloro-4-fluorophenyl)-2-methylpropionamide (945969-63-1) → 4-(2-chloro-4-fluorophenyl)-2,2-dimethyl-7-nitro-2H-1,4-benzoxazin-3(4H)-one (945969-64-2)

Guidance literature:

With pyridine; copper(l) iodide; potassium carbonate; at 100 ℃;

upstream raw materials:

ethyl 2-(2-bromo-5-nitrophenoxy)-2-methylpropionate

2-chloro-4-fluoroaniline

Downstream raw materials:

4-(2-chloro-4-fluorophenyl)-2,2-dimethyl-7-nitro-2H-1,4-benzoxazin-3(4H)-one

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