tris[4-({4-[S-(trifluoromethyl)-N-(acyl)sulfinimidoyl]phenyl}ethynyl)phenyl]amine

Base Information

Chemical Name:tris[4-({4-[S-(trifluoromethyl)-N-(acyl)sulfinimidoyl]phenyl}ethynyl)phenyl]amine
CAS No.:1421132-94-6
Molecular Formula:C₅₁H₃₃F₉N₄O₃S₃
Molecular Weight:1017.03
Hs Code.:

Synonyms:tris[4-({4-[S-(trifluoromethyl)-N-(acyl)sulfinimidoyl]phenyl}ethynyl)phenyl]amine

Suppliers and Price of tris[4-({4-[S-(trifluoromethyl)-N-(acyl)sulfinimidoyl]phenyl}ethynyl)phenyl]amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tris[4-({4-[S-(trifluoromethyl)-N-(acyl)sulfinimidoyl]phenyl}ethynyl)phenyl]amine

Chemical Property:

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Technology Process of tris[4-({4-[S-(trifluoromethyl)-N-(acyl)sulfinimidoyl]phenyl}ethynyl)phenyl]amine

There total 3 articles about tris[4-({4-[S-(trifluoromethyl)-N-(acyl)sulfinimidoyl]phenyl}ethynyl)phenyl]amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1178899-26-7
N-acetyl-S-(p-bromophenyl)-S-(trifluoromethyl)sulfilimine

: 189178-09-4
tri(4-ethynylphenyl)amine

: 1421132-94-6
tris[4-({4-[S-(trifluoromethyl)-N-(acyl)sulfinimidoyl]phenyl}ethynyl)phenyl]amine

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In toluene; at 40 ℃; for 16h; Inert atmosphere;
DOI:10.1002/chem.201103460

Reference yield:

: 4589-43-9
1-bromo-4-[(trifluoromethane)sulfinyl]benzene

: 1421132-94-6
tris[4-({4-[S-(trifluoromethyl)-N-(acyl)sulfinimidoyl]phenyl}ethynyl)phenyl]amine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide; trifluoromethylsulfonic anhydride / 16 h / -15 °C / Inert atmosphere

2: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / toluene / 16 h / 40 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; trifluoromethylsulfonic anhydride; triethylamine; sodium hydroxide; In toluene;
DOI:10.1002/chem.201103460

Reference yield:

: 189178-08-3
N,N',N''-tris-[4-(trimethylsilylethynyl)phenyl]phenylamine

: 1421132-94-6
tris[4-({4-[S-(trifluoromethyl)-N-(acyl)sulfinimidoyl]phenyl}ethynyl)phenyl]amine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / tetrahydrofuran / 35 h / 20 °C / Inert atmosphere

2: bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine / toluene / 16 h / 40 °C / Inert atmosphere

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; sodium hydroxide; In tetrahydrofuran; toluene;
DOI:10.1002/chem.201103460