C₁₆H₁₉NO

Base Information

Chemical Name:C₁₆H₁₉NO
CAS No.:1437311-43-7
Molecular Formula:C₁₆H₁₉NO
Molecular Weight:241.333
Hs Code.:

Synonyms:C₁₆H₁₉NO

Suppliers and Price of C₁₆H₁₉NO

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₁₆H₁₉NO

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₁₆H₁₉NO

There total 7 articles about C₁₆H₁₉NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₁₇NO

: 1437311-43-7
C₁₆H₁₉NO

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 ℃; for 0.5h;
DOI:10.1021/ol4011129

Reference yield:

: 1-(2-(((tert-butyldimethylsilyl)oxy)methyl)phenyl)-3-(trimethylsilyl)prop-2-yn-1-ol

: 1437311-43-7
C₁₆H₁₉NO

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.67 h / 0 °C

1.2: 4 h / 20 °C

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 10 h / 20 °C

3.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 4 h / Reflux

4.1: magnesium sulfate / dichloromethane / 3 h

5.1: sodium tetrahydroborate / methanol / 0.5 h / 0 °C

With sodium tetrahydroborate; tetrabutyl ammonium fluoride; sodium hydride; magnesium sulfate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; mineral oil; 5.1: |Claisen Rearrangement;
DOI:10.1021/ol4011129

Reference yield:

: 1437311-23-3
(2-(1-(allyloxy)prop-2-yn-1-yl)phenyl)methanol

: 1437311-43-7
C₁₆H₁₉NO

Guidance literature:: Multi-step reaction with 3 steps

1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 4 h / Reflux

2: magnesium sulfate / dichloromethane / 3 h

3: sodium tetrahydroborate / methanol / 0.5 h / 0 °C

With sodium tetrahydroborate; magnesium sulfate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In methanol; dichloromethane; ethyl acetate; 3: |Claisen Rearrangement;
DOI:10.1021/ol4011129