3,5-Dinitro-benzoic acid (1S,2S)-1-ethyl-2-(1-ethyl-propoxycarbonyl)-propyl ester

Base Information

Chemical Name:3,5-Dinitro-benzoic acid (1S,2S)-1-ethyl-2-(1-ethyl-propoxycarbonyl)-propyl ester
CAS No.:207788-53-2
Molecular Formula:C₁₈H₂₄N₂O₈
Molecular Weight:396.397
Hs Code.:

Synonyms:3,5-Dinitro-benzoic acid (1S,2S)-1-ethyl-2-(1-ethyl-propoxycarbonyl)-propyl ester

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Chemical Property of 3,5-Dinitro-benzoic acid (1S,2S)-1-ethyl-2-(1-ethyl-propoxycarbonyl)-propyl ester

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Technology Process of 3,5-Dinitro-benzoic acid (1S,2S)-1-ethyl-2-(1-ethyl-propoxycarbonyl)-propyl ester

There total 4 articles about 3,5-Dinitro-benzoic acid (1S,2S)-1-ethyl-2-(1-ethyl-propoxycarbonyl)-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 99-34-3
3,5-dinitrobenzoic acid

: 211621-52-2
1'-ethylpropyl 3-hydroxy-2-methylpentanoate

: 207788-53-2
3,5-Dinitro-benzoic acid (1S,2S)-1-ethyl-2-(1-ethyl-propoxycarbonyl)-propyl ester

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; Ambient temperature;
DOI:10.1055/s-1998-2052

Reference yield:

: 137708-17-9
1'-ethylpropyl-2-methyl-3-oxopentanoate

: 207788-53-2
3,5-Dinitro-benzoic acid (1S,2S)-1-ethyl-2-(1-ethyl-propoxycarbonyl)-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1) 60percent NaH / 1) Et₂O, rt, 2) overnight

2: 1)KH₂PO₄/K₂HPO₄ (pH 6.5), glucose, 2) Ph₃P, DEAD / 1) 30 deg C , 14 h, growing cells of Pichia farinosa IAM 4682, 2) THF

With dipotassium hydrogenphosphate; potassium dihydrogenphosphate; D-glucose; sodium hydride; triphenylphosphine; diethylazodicarboxylate;
DOI:10.1016/S0040-4020(01)89726-X

Reference yield:

: 211621-52-2
1'-ethylpropyl 3-hydroxy-2-methylpentanoate

: 207788-53-2
3,5-Dinitro-benzoic acid (1S,2S)-1-ethyl-2-(1-ethyl-propoxycarbonyl)-propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / CrO₃

2: 1) 60percent NaH / 1) Et₂O, rt, 2) overnight

3: 1)KH₂PO₄/K₂HPO₄ (pH 6.5), glucose, 2) Ph₃P, DEAD / 1) 30 deg C , 14 h, growing cells of Pichia farinosa IAM 4682, 2) THF

With chromium(VI) oxide; dipotassium hydrogenphosphate; potassium dihydrogenphosphate; D-glucose; sodium hydride; triphenylphosphine; diethylazodicarboxylate;
DOI:10.1016/S0040-4020(01)89726-X